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A Ghost Story: Remnant Structures in Corroded Ancient Iron Objects

Published online by Cambridge University Press:  21 March 2011

Michael R. Notis*
Affiliation:
Archaeometallurgy Laboratory Department ofMaterials Science & Engineering Lehigh UniversityBethlehem, PA 18015, USA
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Abstract

The applicability of a broad spectrum of laboratory analytical methods to the study of remnant structures still observable in the corrosion products of ancient iron objects is discussed. These methods range from examination by light optical microscopy and SEM to direct microanalysis using x-ray mapping in EPMA. Samples ranging from low carbon iron to steels to cast iron have been examined and it has been found possible to observe remnant structures and infer fabrication information from the large majority of objects studied. The author thanks the Nathan Rubin-Ida Ladd Foundation for its support.

Type
Research Article
Copyright
Copyright © Materials Research Society 2002

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References

REFERENCES

1. Notis, M.R., Lyman, C.E., Moyer, H., and Cowen, C., in Materials Issues in Art and Archaeology, edited by Sayre, E.V., Vandiver, P.B., Druzik, J., and Stevenson, C., (Mater. Res. Soc. Proc. 123, Pittsburgh, PA, 1988) pp.183192.Google Scholar
2. Pourbaix, M., “Electrochemical Corrosion and Reduction”, Corrosion and Metal Artifacts (NBS Special Publication 479), Brown, B.F.et.al., eds., (Washington, D.C., 1977), pp.116.Google Scholar
3. Had, J., Balcar, J., and Pracharova, H., “Phase Analysis of Rusts by X-ray Diffraction, IR-Spectroscopy and Thermal Analysis”, X-Ray and Neutron Structure Analysis in Materials Science, Plenum Press (1989), pp. 6771.Google Scholar
4. Fontana, M.G., Met.Trans. 1, 32513266. (1970).Google Scholar
5. Cron, C.J., Payer, J.H., and Staehle, R.W., Corrosion, 27, 125. (1971).Google Scholar
6. Felloni, L., Cammarota, G.P., Palombarini, G., and Poli, G., British Corrosion Journal, 13[4], 167172. (1978).Google Scholar
7. Tsubakino, H., Sakai, T., Kim, K.B., Yamakawa, K., Journal of the Society of Materials Science of Japan (Zairyo) 35, 1924. (1986).Google Scholar
8. Giggins, C.S. and Pettit, F.S., Oxidation of Metals, 14, 363413. (1980).Google Scholar
9. Knox, R., Archaeometry, 6, 4346. (1963).Google Scholar
10. Maxwell-Hyslop, K.R., Wheeler, T.S., Maddin, R., and Muhly, J., Levant, X, 112115. (1978).Google Scholar
11. Stech-Wheeler, T., Muhly, J.D., Maxwell-Hyslop, K.R., and Maddin, R., AJA, 85, 245268. (1981).Google Scholar
12. Muhly, J.D., Maddin, P., Stech, T., and Ozgen, E., Anatolian Studies, XXXV, 6784. (1985).Google Scholar
13. Pigott, V., Expedition, 31[2–3], 6779. (1989).Google Scholar
14. Scott, B.G., “Remanent Metal Structures in Corrosion Products from an Early Mediaeval Iron Knife”, Irish Archaeological Research Forum, Volume III [Part 2], (1976), pp.6164.Google Scholar
15. Scott, B., “Retrieval of Technological Information from Corrosion Products on Early Wrought Iron Artifacts”, Conservation Today, 30th Anniversary Conf. of the United Kingdom Institute for Conservation of Historic and Artistic Works (1988), pp.814.Google Scholar
16. Scott, B.G., “Methods of Conserving Early Iron Objects”, Archaeometallurgy of Iron, Pleiner, R., ed., (Prague, 1989), pp.1016.Google Scholar
17. Pigott, V.C., McGovern, P.E., and Notis, M.R., MASCA Journal, 2[2], 3539. (1982).Google Scholar
18. Murata, T. and Sasaki, M., “Rust Analysis of the Inariyama Sword”, Microbeam Analysis-1984, Romig, A.D. and Goldstein, J.I., eds., (1984), pp.257260.Google Scholar
19. Agrawal, O.P., Narain, H., and Prakash, J., “Metallographic Studies of Iron Artifacts of Domestic Use, Tools & Weapons From Khairadih (100–400. A.D.), Uttar Pradesh”, Role of Chemistry in Archaeology, Ganorkar, M.C. and Rao, N. Rama, eds., (Hyderabad, 1991), pp.103111.Google Scholar
20. Agrawal, O.P., Narain, H., Prakash, J. and Joshi, G.P., “Technical Studies of Iron Artifacts From Dwarka (Mahabharta Period) India”, Papers Presented at the March 1990 Conference of the Historical Metallurgy Society, Lang, J., ed., (1990), pp.4346,Google Scholar
21. Dotan, T., Erets-Yisra'el, 20 (Yigal Yadin Memorial Volume), 154163. (1989)Google Scholar
22. Dotan, T., Gitin, S., Qadmaniot, 27[1–2], 228. (1994)Google Scholar
23. Dotan, T., “Tel Miqne-Ekron:The Aegean Affinities of the Sea Peoples' (Philistines') Settlement in Canaan in Iron Age I”, Recent Excavations in Israel-A View to the West, Gitin, S,ed., (1995), pp.4159.Google Scholar
24. Lyman, C.E., Microscopy: The Key Research Tool, 22[1], 19. (1992)Google Scholar
25. Bright, D.S. and Marinenko, R.B., Microscopy: The Key Research Tool, 22[1], 2128. (1992)Google Scholar