Hostname: page-component-77c89778f8-vpsfw Total loading time: 0 Render date: 2024-07-21T16:14:46.114Z Has data issue: false hasContentIssue false

Fracture of Laminated and In Situ Niobium Silicide-Niobium Composites

Published online by Cambridge University Press:  10 February 2011

J. D. Rigney*
Affiliation:
The Case School of Engineering, Department of Materials Science and Engineering, Case Western Reserve University, Cleveland, OH 44106 U.S.A.
Get access

Abstract

The mechanisms contributing to the fracture resistance of refractory metal intermetallic composites containing a BCC metallic phase (niobium) were investigated using model Nb-Si laminates and in situ composites. The controlling influence of ductile phase yield strength and fracture behavior were investigated by varying laminate processing parameters, and/or altering temperatures and applied strain rates during fracture experiments on all materials. The fracture behavior of “ductile” constituents were found to be influenced by phase grain size, solid solution content, constraint (as influenced by interfacial bond strengths), and the testing condition (high strain rates and low temperatures). The measured fracture resistance, when compared to theoretical models, was shown to be controlled by the “toughness” of the “ductile” phase and independent of the fracture behavior promoted (cleavage and ductile). The loss in ductility due to cleavage by high constraint, high strain rates and/or low temperatures was compensated by high yield and cleavage fracture stresses in order to provide a level of toughening similar to that contributed by ligaments which failed with lower yield stresses and greater strains.

Type
Research Article
Copyright
Copyright © Materials Research Society 1996

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1. Fleischer, R.L.: J. Mater. Sci., 1987, vol.22, pp. 2281–8.Google Scholar
2. Subramanian, P.R., Mendiratta, M.G., and Dimiduk, D.M.: JOM, 1996, vol.48, pp. 33–8.Google Scholar
3. Dimiduk, D.M., Subramanian, P.R., and Mendiratta, M.G.: ActaMetall. Sinica, 1995, vol.8, pp. 519–30.Google Scholar
4. Mendiratta, M.G., Lewandowski, J.J., and Dimiduk, D.M.: Metall. Trans. A, 1991, vol.22A, pp. 1573–83.Google Scholar
5. Nekkanti, R.M. and Dimiduk, D.M.: Intermetallic Matrix Composites, Mater. Res. Soc. Symp. Proc., vol.194, Materials Research Society, Pittsburgh, PA, 1990, pp. 175.Google Scholar
6. Kajuch, J., Rigney, J.D., and Lewandowski, J.J.: Mater. Sci. Eng. A, 1992, vol. A155, pp. 5965.Google Scholar
7. Lewandowski, J.J., Dimiduk, D.M., Kerr, W., and Mendiratta, M.G.: High Temperature Composite Materials, Mater. Res. Soc. Symp. Proc, vol.120, Materials Research Society, Pittsburgh, PA, 1989, pp. 103.Google Scholar
8. Mendiratta, M.G. and Dimiduk, D.M.: Scr. Metall. Mater., 1991, vol.25, pp. 237–42.Google Scholar
9. Mataga, P.A.: Acta Metall., 1989, vol.37, pp. 3349–59.Google Scholar
10. Krstic, V.D., Nicholson, P.S., and Hoagland, R.G.: J. Am. Ceram. Soc., 1981, vol.64, 499.Google Scholar
11. Ashby, M.F., Blunt, F.J., and Bannister, M.: Acta Metall., 1989, vol.37, pp. 1847–57.Google Scholar
12. Rigney, J.D. and Lewandowski, J.J.: Metall. Mater. Trans. A, 1996, in press.Google Scholar
13. Kajuch, J., Short, J., and Lewandowski, J.J.: Acta Metall. Mater., 1995, vol.43, pp. 1955–67.Google Scholar
14. Short, J.A.: Master's Thesis, Case Western Reserve University, Cleveland, OH, 1994.Google Scholar
15. Bewlay, B.P., Jackson, M.R., Lipsitt, H.A., Reeder, W.J., and Sutcliff, J.A.: 1996 AFOSR Report F49620-93-C-0007. General Electric Corporate R&D, Schnectady, NY, 1996.Google Scholar
16. Standard E-399. Annual Book ofASTM Standards. Vol.03.01. American Society for Testing and Materials, Philadelphia, PA (1988), p. 480.Google Scholar
17. Adams, M.A., Roberts, A.C., and Smallman, R.E.: Acta Metall., 1960, vol.8, pp. 328–37.Google Scholar
18. Johnson, A.A.: Acta Metall., 1960, vol.8, pp. 737–40.Google Scholar
19. Mendiratta, M.G., Goetz, R., Dimiduk, D.M., and Lewandowski, J.J.: Metall. Mater. Trans. A, 1995, vol.26A, pp. 1767–77.Google Scholar
20. Knott, J.F.: Fundamentals of Fracture Mechanics, Butterworths: London, England, 1973.Google Scholar
21. Cottrell, A.H.: Trans. Metall. Soc. AIME, 1958, vol.212, pp. 192202.Google Scholar
22. Samant, A.V. and Lewandowski, J.J.: Metall. Mater. Trans. A, 1996, in press.Google Scholar
23. Mendiratta, M.G. and Dimiduk, D.M.: Metall. Trans. A, 1993, vol.24A, pp. 501–4.Google Scholar
24. Rigney, J.D.: Ph.D. Thesis, Case Western Reserve University, Cleveland, OH, 1994.Google Scholar
25. Briggs, T.L. and Campbell, J.D.: Acta Metall., 1972, vol.20, pp. 711–24.Google Scholar
26. Sargent, G.A.: Acta Metall., 1965, vol.13, pp. 663–71.Google Scholar
27. Imgram, A.G., Holden, F.C., Ogden, H.R., and Jaffee, R.I.: Trans. Metall. Soc. AIME, 1961, vol.221, pp. 517–26.Google Scholar
28. Imgram, A.G., Bartlett, E.S., and Ogden, H.R.: Trans. Metall. Soc. AIME, 1963, vol.227, pp. 131–6.Google Scholar
29. Mincher, A.L. and Sheeley, W.F.: Trans. Metall. Soc. AIME, 1961, vol.221, pp. 1925.Google Scholar
30. Begley, R.T. and Bechtold, J.H.: J. Less-Common Met., 1961, vol.3, pp. 112.Google Scholar