Hostname: page-component-76fb5796d-25wd4 Total loading time: 0 Render date: 2024-04-27T00:52:01.286Z Has data issue: false hasContentIssue false

The Effect of Surface Finish on the Dislocation Density in Sublimation grown SiC Layers

Published online by Cambridge University Press:  21 March 2011

E. K. Sanchez
Affiliation:
Department of Materials Science & Engineering, Carnegie Mellon University, 5000 Forbes Avenue, Pittsburgh, PA 15213, USA.
J. Liu
Affiliation:
Department of Materials Science & Engineering, Carnegie Mellon University, 5000 Forbes Avenue, Pittsburgh, PA 15213, USA.
W. M. Vetter
Affiliation:
Department of Materials Science & Engineering, State University of New York, Stony Brook, NY 11794, USA.
M. Dudley
Affiliation:
Department of Materials Science & Engineering, State University of New York, Stony Brook, NY 11794, USA.
R. Bertke
Affiliation:
Air Force Research Laboratory, Materials and Manufacturing Directorate, AFRL/MLP, Wright Patterson AFB, OH 45433
W. C. Mitchel
Affiliation:
Air Force Research Laboratory, Materials and Manufacturing Directorate, AFRL/MLP, Wright Patterson AFB, OH 45433
M. Skowronski
Affiliation:
Department of Materials Science & Engineering, Carnegie Mellon University, 5000 Forbes Avenue, Pittsburgh, PA 15213, USA.
Get access

Abstract

The effect of the seed surface finish on the dislocation density of sublimation grown silicon carbide was investigated. Growth on seeds that were polished down to 1 μm diamond paste resulted in the nucleation of threading screw dislocations in a density of 106 cm−2 and threading edge dislocations in densities of 107 cm−2. Following the mechanical polish of the seeds with a hydrogen etch or chemo-mechanical polish prior to growth resulted in the screw dislocation density decreasing by four orders of magnitude and the threading edge dislocation density dropping two orders of magnitude. Using the dislocations density and the hydrogen etch rate, the depth of damage in mechanically damaged seeds was determined to be between 400 and 1000 Å.

Type
Research Article
Copyright
Copyright © Materials Research Society 2001

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Hobgood, D., Brady, M., Brixius, W., Fechko, G., Glass, R., Henshall, D., Jenny, J., Leonard, R., Malta, D., Muller, St. G., Tsvetkov, V., Carter, C. H. Jr, Mater. Sci. Forum 338–342, 3 (2000).Google Scholar
2. Glass, R. C., Henshall, D., Tsvetkov, V. F., Carter, C. H. Jr, Phys. Stat. Sol. (b) 202, 149 (1997).Google Scholar
3. Takahashi, J., Ohtani, N., Kanaya, M., J. Cryst. Growth 167, 596 (1996).Google Scholar
4. Neudeck, P. G., Huang, W., Dudley, M., Mat. Res. Soc. Symp. Proc. 483, 285 (1998).Google Scholar
5. Ha, S., Nuhfer, N. T., Rohrer, G. S., Graef, M. De, Skowronski, M., J. Elec. Mat. 29, L5 (2000).Google Scholar
6. Dudley, M., Huang, X. R., Huang, W., Powell, A., Wang, S., Neudeck, P., Skowronski, M., Appl. Phys. Letters 75, 784 (1999).Google Scholar
7. Hallen, C., Owman, F., Martensson, P., Ellison, A., Konstantinov, A., Kordina, O., Janzen, E., J. Cryst. Growth 181, 241 (1997).Google Scholar
8. Powell, J. A., Larkin, D. J., Phys. Stat. Sol. (b) 202, 529 (1997).Google Scholar
9. Everson, W. J., Snyder, D. W., Heydemann, V. D., Mater. Sci. Forum 338–342, 837 (2000).Google Scholar
10. Ramachandran, V., Brady, M. F., Smith, A. R., Feenstra, R. M., Greve, D. W., J. Elec. Mat. 27, 308 (1998).Google Scholar
11. Zhou, L., Audurier, V., Pirouz, P., Powell, J. A., J. Electrochem. Soc. 144, L161 (1997).Google Scholar
12. Saddow, S. E., Schattner, T. E., Brown, J., Grazulis, L., Mahalingham, K., Landis, G., Bertke, R., Mitchel, W. C., submitted to J. Elec. Mat. (2000).Google Scholar
13. Qian, W., Skowronski, M., Augustine, G., Glass, R. C., Hobgood, H. McD., Hopkins, R. H., J. Electrochem. Soc. 142, 4290 (1995).Google Scholar
14. Barret, D. L., Seidensticker, R. G., Gaida, W., Hopkins, R. H., Choyke, W. J., J. Cryst. Growth 109, 12 (1991).Google Scholar
15. Sanchez, E. K., Heydemann, V. D., Snyder, D. W., Rohrer, G. S., Skowronski, M., J. Elec. Mat. 29, 347 (2000).Google Scholar
16. Takahashi, J., Ohtani, N., Kanaya, M., J. Cryst. Growth 167, 596 (1996).Google Scholar