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RBS and PIXE Analysis of Alteration Layers on Waste Glass in a Leaching Test Under Reducing Condition

Published online by Cambridge University Press:  25 February 2011

Kaoru Sasakawa
Affiliation:
Kobelco Research Institute, Inc., Takatsukadai, Nishi-ku, Kobe 651-22, Japan
Tsuyoshi Imakita
Affiliation:
Kobelco Research Institute, Inc., Takatsukadai, Nishi-ku, Kobe 651-22, Japan
Ryutaro Wada
Affiliation:
Kobe Steel, Ltd., Wakinohama-cho, Chuo-ku, Kobe 651, Japan
Fumio Matsuda
Affiliation:
Kobe Steel, Ltd., Wakinohama-cho, Chuo-ku, Kobe 651, Japan
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Abstract

A corrosion test of model waste glass was carried out with and without a carbon steel under reducing condition in a glove box purged with nitrogen gas, and then the characteristics of alteration layers of the glass were examined.

On the glass surfaces corroded under reducing condition with carbon steel, a thick precipitated layer was observed by Scanning Electron Microscopy (SEM). In this layer concentrated iron was observed by Particle Induced X-ray Emission Spectrometry (PIXE) and Rutherford Backseattering Spectrometry (RBS). Such a thick precipitated layer was not observed on the corroded glass under oxidizing conditions with and without carbon steel and reducing condition without carbon steel.

Type
Research Article
Copyright
Copyright © Materials Research Society 1994

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References

1 Power Reactor and Nuclear Fuel Development, Co., PNC TO410 93-012 (H3 report), 1992.Google Scholar

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