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Advanced Cryo-FIB Specimen Preparation and Handling of Environmentally Sensitive Materials for APT Analysis

Published online by Cambridge University Press:  30 July 2020

Daniel Perea*
Affiliation:
Pacific Northwest National Laboratory, Richland, Washington, United States

Abstract

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Type
Physical Sciences Tutorial: Advanced Cryo-FIB Specimen Preparation and Handling of Environmentally Sensitive Materials for APT and TEM Analysis
Copyright
Copyright © Microscopy Society of America 2020

References

Zachman, M.J., de Jonge, N., Fischer, R., Jungjohann, K.L., and Perea, D.E., Cryogenic specimens for nanoscale characterization of solid-liquid interfaces. MRS Bulletin, 2019. 44(12): p. 949955.10.1557/mrs.2019.289CrossRefGoogle Scholar
Zachman, M.J., Asenath-Smith, E., Estroff, L.A., and Kourkoutis, L.F., Site-Specific Preparation of Intact Solid-Liquid Interfaces by Label-Free In Situ Localization and Cryo-Focused Ion Beam Lift-Out. Microscopy and Microanalysis, 2016. 22(6): p. 13381349.10.1017/S1431927616011892CrossRefGoogle ScholarPubMed
Perea, D.E., Gerstl, S.S.A., Chin, J., Hirschi, B., and Evans, J.E., An environmental transfer hub for multimodal atom probe tomography. Advanced Structural and Chemical Imaging, 2017. 3(1): p. 12.10.1186/s40679-017-0045-2CrossRefGoogle ScholarPubMed
Schreiber, D.K., Perea, D.E., Ryan, J.V., Evans, J.E., and Vienna, J.D., A method for site-specific and cryogenic specimen fabrication of liquid/solid interfaces for atom probe tomography. Ultramicroscopy, 2018. 194: p. 8999.10.1016/j.ultramic.2018.07.010CrossRefGoogle ScholarPubMed
Perea, D.E., Schreiber, D.K., Ryan, J.V., Wirth, M.G., Deng, L., Lu, X., Du, J., and Vienna, J.D., Tomographic mapping of the nanoscale water-filled pore structure in corroded borosilicate glass. npj Materials Degradation, 2020. in press.10.1038/s41529-020-0110-5CrossRefGoogle Scholar