Hostname: page-component-cd9895bd7-p9bg8 Total loading time: 0 Render date: 2024-12-22T05:45:35.240Z Has data issue: false hasContentIssue false
  • English
  • Français

Instrumented indentation microscope: A powerful tool for the mechanical characterization in microscales

Published online by Cambridge University Press:  03 March 2011

M. Sakai ,
N. Hakiri  and
T. Miyajima
M. Sakai*
Affiliation:
Department of Materials Science, Toyohashi University of Technology, Tempaku-cho, Toyohashi 441-8580, Japan
N. Hakiri
Affiliation:
Department of Materials Science, Toyohashi University of Technology, Tempaku-cho, Toyohashi 441-8580, Japan
T. Miyajima
Affiliation:
Research Institute of Instrumentation Frontier, National Institute of Advanced Industrial Science and Technology (AIST), Shimo-shidami, Moriyama-ku, Nagoya 463-8560, Japan
*
a) Address all correspondence to this author. e-mail: msakai@tutms.tut.ac.jp This author was an editor of this journal during the review and decision stage. For the JMR policy on review and publication of manuscripts authored by editors, please refer to http://www.mrs.org/publications/jmr/policy.html.
Get access

Abstract

An instrumented indentation microscope was constructed and applied to the measurements of the Meyer hardness and the elastic modulus of several engineering materials ranging from ductile metals to brittle ceramics. Because of the in situ optical observation and determination of the indentation contact area that is synchronized to the indentation load versus depth relation, the mechanical properties determined on the indentation microscope are precise and reliable without any undesirable approximations and assumptions required for estimating the contact area. It is also demonstrated that the instrumented indentation microscope is capable of determining in a quantitative manner the in situ contact profiles of impression (sinking-in/piling-up profiles). The present work suggests that the instrumented indentation microscope will be a powerful tool in the science and engineering of indentation contact mechanics.

Keywords

Elastic propertiesHardnessOptical
Type
Articles
Information
Journal of Materials Research , Volume 21 , Issue 9 , September 2006 , pp. 2298 - 2303
Copyright
Copyright © Materials Research Society 2006

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1Oliver, W.C. and Pharr, G.M.: Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology. J. Mater. Res. 19, 3 (2004).CrossRefGoogle Scholar
2Cook, R.F. and Pharr, G.M.: Direct observation and analysis of indentation cracking in glasses and ceramics. J. Am. Ceram. Soc. 73, 787 (1990).CrossRefGoogle Scholar
3Cook, R.F. and Liniger, E.G.: Kinetics of indentation cracking in glass. J. Am. Ceram. Soc. 76, 1096 (1993).CrossRefGoogle Scholar
4Lee, C.S., Kim, D.K., Sánchez, J., Miranda, P., Pajares, A., and Lawn, B.R.: Rate effects in critical loads for radial cracking in ceramic coatings. J. Am. Ceram. Soc. 85, 2019 (2002).CrossRefGoogle Scholar
5Sakai, M. and Nakano, Y.: Elastoplastic load-depth hysteresis in pyramidal indentation. J. Mater. Res. 17, 2161 (2002).CrossRefGoogle Scholar
6Oliver, W.C. and Pharr, G.M.: An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. J. Mater. Res. 7, 1564 (1992).CrossRefGoogle Scholar
7Cheng, Y-T. and Cheng, C-M.: Scaling, dimensional analysis, and indentation measurements. Mater. Sci. Eng., R 44, 91 (2004).CrossRefGoogle Scholar
8Chen, X. and Vlassak, J.J.: Numerical study on the measurement of thin film mechanical properties by means of nanoindentation. J. Mater. Res. 16, 2974 (2001).CrossRefGoogle Scholar
9Saha, R. and Nix, W.D.: Effects of the substrate on the determination of thin film mechanical properties by nanoindentation. Acta Mater. 50, 23 (2002).CrossRefGoogle Scholar
10Tsui, T.Y., Ross, C.A., and Pharr, G.M.: A method for making substrate-independent hardness measurements of soft metallic films on hard substrates by nanoindentation. J. Mater. Res. 18, 1383 (2003).CrossRefGoogle Scholar
11Han, S.M., Saha, R., and Nix, W.D.: Determining hardness of thin film in elastically mismatched film-on-substrate systems using nanoindentation. Acta Mater. 54, 1571 (2006).CrossRefGoogle Scholar
12Feng, C. and Kang, B.S-J.: A transparent indenter measurement method for mechanical propertiy evaluation. Exper. Mech. 46, 91 (2006).CrossRefGoogle Scholar
13Miyajima, T. and Sakai, M.: Optical indentation microscope—A new family of instrumented indentation testing. Philos. Mag. A (in press).Google Scholar
14Johnson, K.L.: Contact Mechanics (Cambridge University Press, Cambridge, UK, 1985).Google Scholar
15Sakai, M.: Energy principle of the indentation-induced inelastic surface deformation and hardness of brittle materials. Acta Metall. Mater. 41, 1751 (1993).CrossRefGoogle Scholar
16Sakai, M., Shimizu, S., and Ishikawa, T.: The indentation load-depth curve of ceramics. J. Mater. Res. 14, 1471 (1999).CrossRefGoogle Scholar
17Sakai, M.: The Meyer hardness: A measure for plasticity? J. Mater. Res. 14, 3630 (1999).CrossRefGoogle Scholar
18Sakai, M., Akatsu, T., Numata, S., and Matsuda, K.: Linear strain hardening in elastoplastic indentation contact. J. Mater. Res. 18, 2087 (2003).CrossRefGoogle Scholar
19Shorshorov, M.Kh., Bulychev, S.I., and Alekhin, V.P.: Work of plastic and elastic deformation during indenter indentation. Sov. Phys. Doki. 26, 769 (1981).Google Scholar
20Pharr, G.M., Oliver, W.C., and Brotzen, F.R.: On the generality of the relationship among contact stiffness, contact area, and elastic modulus during indentation. J. Mater. Res. 7, 613 (1992).CrossRefGoogle Scholar
21Field, J.S. and Swain, M.V.: Determining the mechanical properties of small volumes of materials from submicron spherical indentation. J. Mater. Res. 10, 101 (1995).CrossRefGoogle Scholar