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An overview of interface-dominated deformation mechanisms in metallic nanocomposites elucidated using in situ straining in a TEM

Published online by Cambridge University Press:  07 March 2019

Yuchi Cui
Affiliation:
Department of Materials Science and Engineering, University of Michigan, Ann Arbor, Michigan 48109, USA
Nan Li
Affiliation:
Center for Integrated Nanotechnologies, Los Alamos National Laboratory, Los Alamos, New Mexico 87545, USA
Amit Misra
Affiliation:
Department of Materials Science and Engineering, University of Michigan, Ann Arbor, Michigan 48109, USA; and Department of Mechanical Engineering, University of Michigan, Ann Arbor, Michigan 48109, USA
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Abstract

Nanostructured multiphase metallic materials present extraordinary properties, such as high strength, enhanced fatigue and radiation resistance, and thermal stability, compared to conventional bulk metallic materials. Previous research studies have shown that their deformation and fracture behavior are dominated by defect interactions at internal interfaces. In situ straining, including nanoindentation, compression, and tension, in a transmission electron microscope (TEM) has emerged as a powerful tool to investigate the physics of defect–interface interactions at the nano-scale and even atomic scale. The mechanistic insights gained from these experiments coupled with dislocation theory and atomistic modeling has helped develop a fundamental understanding of the mechanical properties. In this article, through some recent investigations on observing dislocation and interface activities, crack propagation, and nanopillar compression, we present current progress in utilizing in situ TEM straining to examine interface-dominated deformation mechanisms.

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Invited Feature Paper - REVIEW
Copyright
Copyright © Materials Research Society 2019 

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Footnotes

b)

This author was an editor of this journal during the review and decision stage. For the JMR policy on review and publication of manuscripts authored by editors, please refer to http://www.mrs.org/editor-manuscripts/.

This paper has been selected as an Invited Feature Paper.

References

Clemens, B.M., Kung, H., and Barnett, S.A.: Structure and strength of multilayers. MRS Bull. 24, 2026 (1999).CrossRefGoogle Scholar
Anderson, P.M., Foecke, T., and Hazzledine, P.M.: Dislocation-based deformation mechanisms in metallic nanolaminates. MRS Bull. 24, 2733 (1999).CrossRefGoogle Scholar
Misra, A., Demkowicz, M., Zhang, X., and Hoagland, R.: The radiation damage tolerance of ultra-high strength nanolayered composites. JOM 59, 6265 (2007).CrossRefGoogle Scholar
Wang, Y-C., Misra, A., and Hoagland, R.: Fatigue properties of nanoscale Cu/Nb multilayers. Scr. Mater. 54, 15931598 (2006).CrossRefGoogle Scholar
Primorac, M-M., Abad, M.D., Hosemann, P., Kreuzeder, M., Maier, V., and Kiener, D.: Elevated temperature mechanical properties of novel ultra-fine grained Cu–Nb composites. Mater. Sci. Eng., A 625, 296302 (2015).CrossRefGoogle Scholar
Hoagland, R.G., Kurtz, R.J., and Henager, C.H. Jr.: Slip resistance of interfaces and the strength of metallic multilayer composites. Scr. Mater. 50, 775779 (2004).CrossRefGoogle Scholar
Misra, A., Hirth, J.P., and Hoagland, R.G.: Length-scale-dependent deformation mechanisms in incoherent metallic multilayered composites. Acta Mater. 53, 48174824 (2005).CrossRefGoogle Scholar
Wang, J. and Misra, A.: An overview of interface-dominated deformation mechanisms in metallic multilayers. Curr. Opin. Solid State Mater. Sci. 15, 2028 (2011).CrossRefGoogle Scholar
Bhattacharyya, D., Mara, N.A., Dickerson, P., Hoagland, R.G., and Misra, A.: Transmission electron microscopy study of the deformation behavior of Cu/Nb and Cu/Ni nanoscale multilayers during nanoindentation. J. Mater. Res. 24, 12911302 (2009).CrossRefGoogle Scholar
Hoagland, R.G., Mitchell, T.E., Hirth, J.P., and Kung, H.: On the strengthening effects of interfaces in multilayer fee metallic composites. Philos. Mag. A 82, 643664 (2002).Google Scholar
Wang, J., Misra, A., Hoagland, R., and Hirth, J.: Slip transmission across fcc/bcc interfaces with varying interface shear strengths. Acta Mater. 60, 15031513 (2012).CrossRefGoogle Scholar
Hoagland, R.G., Hirth, J.P., and Misra, A.: On the role of weak interfaces in blocking slip in nanoscale layered composites. Philos. Mag. 86, 35373558 (2006).CrossRefGoogle Scholar
Cui, Y., Derby, B., Li, N., Mara, N.A., and Misra, A.: Suppression of shear banding in high-strength Cu/Mo nanocomposites with hierarchical bicontinuous intertwined structures. Mater. Res. Lett. 6, 184190 (2018).CrossRefGoogle Scholar
Wilsdorf, H.: Apparatus for the deformation of foils in an electron microscope. Rev. Sci. Instrum. 29, 323324 (1958).CrossRefGoogle Scholar
Yu, Q., Legros, M., and Minor, A.: In situ TEM nanomechanics. MRS Bull. 40, 6270 (2015).CrossRefGoogle Scholar
Haque, M.A. and Saif, M.T.A.: In situ tensile testing of nano-scale specimens in SEM and TEM. Exp. Mech. 42, 123128 (2002).CrossRefGoogle Scholar
Li, N., Wang, J., Mao, S., and Wang, H.: In situ nanomechanical testing of twinned metals in a transmission electron microscope. MRS Bull. 41, 305313 (2016).CrossRefGoogle Scholar
Oh, S.H., Legros, M., Kiener, D., and Dehm, G.: In situ observation of dislocation nucleation and escape in a submicrometre aluminium single crystal. Nat. Mater. 8, 95 (2009).CrossRefGoogle Scholar
Clouet, E., Caillard, D., Chaari, N., Onimus, F., and Rodney, D.: Dislocation locking versus easy glide in titanium and zirconium. Nat. Mater. 14, 931 (2015).CrossRefGoogle ScholarPubMed
Wang, J., Li, N., Anderoglu, O., Zhang, X., Misra, A., Huang, J.Y., and Hirth, J.P.: Detwinning mechanisms for growth twins in face-centered cubic metals. Acta Mater. 58, 22622270 (2010).CrossRefGoogle Scholar
Ye, J., Mishra, R.K., Sachdev, A.K., and Minor, A.M.: In situ TEM compression testing of Mg and Mg–0.2 wt% Ce single crystals. Scr. Mater. 64, 292295 (2011).CrossRefGoogle Scholar
Morrow, B.M., McCabe, R.J., Cerreta, E.K., and Tomé, C.N.: In situ TEM observation of twinning and detwinning during cyclic loading in Mg. Metall. Mater. Trans. A 45, 3640 (2014).CrossRefGoogle Scholar
Wang, J., Zeng, Z., Weinberger, C.R., Zhang, Z., Zhu, T., and Mao, S.X.: In situ atomic-scale observation of twinning-dominated deformation in nanoscale body-centred cubic tungsten. Nat. Mater. 14, 594 (2015).CrossRefGoogle ScholarPubMed
Yu, Q., Shan, Z-W., Li, J., Huang, X., Xiao, L., Sun, J., and Ma, E.: Strong crystal size effect on deformation twinning. Nature 463, 335 (2010).CrossRefGoogle ScholarPubMed
Li, N., Wang, J., Misra, A., Zhang, X., Huang, J.Y., and Hirth, J.P.: Twinning dislocation multiplication at a coherent twin boundary. Acta Mater. 59, 59895996 (2011).CrossRefGoogle Scholar
, M., Ibarra, A., Caillard, D., and San Juan, J.: Stress-induced phase transformations studied by in-situ transmission electron microscopy. J. Phys.: Conf. Ser., 240, 012002 (2010).Google Scholar
Ma, X., Guo, X., Fu, M., and Qiao, Y.: In situ TEM observation of hcp-Ti to fcc-Ti phase transformation in Nb–Ti–Si based alloys. Mater. Charact. 142, 332339 (2018).CrossRefGoogle Scholar
Liu, Y., Karaman, I., Wang, H., and Zhang, X.: Two types of martensitic phase transformations in magnetic shape memory alloys by in situ nanoindentation studies. Adv. Mater. 26, 38933898 (2014).CrossRefGoogle ScholarPubMed
Jiang, B., Tadaki, T., Mori, H., and Hsu, T.Y.: In situ TEM observation of γ → ε martensitic transformation during tensile straining in an Fe–Mn–Si shape memory alloy. Mater. Trans., JIM 38, 10721077 (1997).CrossRefGoogle Scholar
Ohmura, T., Minor, A., Stach, E., and Morris, J.: Dislocation–grain boundary interactions in martensitic steel observed through in situ nanoindentation in a transmission electron microscope. J. Mater. Res. 19, 36263632 (2004).CrossRefGoogle Scholar
Lee, T., Robertson, I., and Birnbaum, H.: An in situ transmission electron microscope deformation study of the slip transfer mechanisms in metals. Metall. Trans. A 21, 24372447 (1990).CrossRefGoogle Scholar
Lee, T., Robertson, I., and Birnbaum, H.: TEM in situ deformation study of the interaction of lattice dislocations with grain boundaries in metals. Philos. Mag. A 62, 131153 (1990).CrossRefGoogle Scholar
De Hosson, J.T.M., Soer, W.A., Minor, A.M., Shan, Z., Stach, E.A., Syed Asif, S.A., and Warren, O.L.: In situ TEM nanoindentation and dislocation–grain boundary interactions: A tribute to David Brandon. J. Mater. Sci. 41, 77047719 (2006).CrossRefGoogle Scholar
Kiener, D., Hosemann, P., Maloy, S., and Minor, A.: In situ nanocompression testing of irradiated copper. Nat. Mater. 10, 608 (2011).CrossRefGoogle ScholarPubMed
Dillon, S.J., Bufford, D.C., Jawaharram, G.S., Liu, X., Lear, C., Hattar, K., and Averback, R.S.: Irradiation-induced creep in metallic nanolaminates characterized by in situ TEM pillar nanocompression. J. Nucl. Mater. 490, 5965 (2017).CrossRefGoogle Scholar
Jin, M., Minor, A., Stach, E., and Morris, J. Jr.: Direct observation of deformation-induced grain growth during the nanoindentation of ultrafine-grained Al at room temperature. Acta Mater. 52, 53815387 (2004).CrossRefGoogle Scholar
Gouldstone, A., Chollacoop, N., Dao, M., Li, J., Minor, A., and Shen, Y.: Indentation across size scales and disciplines: Recent developments in experimentation and modeling. Acta Mater. 55, 40154039 (2007).CrossRefGoogle Scholar
Minor, A.M., Lilleodden, E.T., Stach, E.A., and Morris, J.W.: Direct observations of incipient plasticity during nanoindentation of Al. J. Mater. Res. 19, 176182 (2011).CrossRefGoogle Scholar
Legros, M., Gianola, D.S., and Hemker, K.J.: In situ TEM observations of fast grain-boundary motion in stressed nanocrystalline aluminum films. Acta Mater. 56, 33803393 (2008).CrossRefGoogle Scholar
Soer, W., De Hosson, J.T.M., Minor, A., Morris, J. Jr., and Stach, E.: Effects of solute Mg on grain boundary and dislocation dynamics during nanoindentation of Al–Mg thin films. Acta Mater. 52, 57835790 (2004).CrossRefGoogle Scholar
Eftink, B.P., Li, A., Szlufarska, I., Mara, N.A., and Robertson, I.M.: Deformation response of AgCu interfaces investigated by in situ and ex situ TEM straining and MD simulations. Acta Mater. 138, 212223 (2017).CrossRefGoogle Scholar
Foecke, T. and Van Heerden, D.: Experimental observations of deformation mechanisms in metallic nanolaminates. Chem. Phys. Nanostruct. Relat. Non-Equilib. Mater., 193200 (1997).Google Scholar
Freund, L.: The driving force for glide of a threading dislocation in a strained epitaxial layer on a substrate. J. Mech. Phys. Solids 38, 657679 (1990).CrossRefGoogle Scholar
Misra, A., Hirth, J.P., and Kung, H.: Single-dislocation-based strengthening mechanisms in nanoscale metallic multilayers. Philos. Mag. A 82, 29352951 (2002).CrossRefGoogle Scholar
Li, N., Wang, J., Misra, A., and Huang, J.Y.: Direct observations of confined layer slip in Cu/Nb multilayers. Microsc. Microanal. 18, 11551162 (2012).CrossRefGoogle ScholarPubMed
Zhang, J.Y., Lei, S., Liu, Y., Niu, J.J., Chen, Y., Liu, G., Zhang, X., and Sun, J.: Length scale-dependent deformation behavior of nanolayered Cu/Zr micropillars. Acta Mater. 60, 16101622 (2012).CrossRefGoogle Scholar
Li, Y.P., Zhu, X.F., Tan, J., Wu, B., Wang, W., and Zhang, G.P.: Comparative investigation of strength and plastic instability in Cu/Au and Cu/Cr multilayers by indentation. J. Mater. Res. 24, 728735 (2011).CrossRefGoogle Scholar
Han, W., Carpenter, J., Wang, J., Beyerlein, I., and Mara, N.: Atomic-level study of twin nucleation from face-centered-cubic/body-centered-cubic interfaces in nanolamellar composites. Appl. Phys. Lett. 100, 011911 (2012).CrossRefGoogle Scholar
Zheng, S.J., Beyerlein, I.J., Wang, J., Carpenter, J.S., Han, W.Z., and Mara, N.A.: Deformation twinning mechanisms from bimetal interfaces as revealed by in situ straining in the TEM. Acta Mater. 60, 58585866 (2012).CrossRefGoogle Scholar
Lu, L., Shen, Y., Chen, X., Qian, L., and Lu, K.: Ultrahigh strength and high electrical conductivity in copper. Science 304, 422426 (2004).CrossRefGoogle ScholarPubMed
Lu, L., Chen, X., Huang, X., and Lu, K.: Revealing the maximum strength in nanotwinned copper. Science 323, 607610 (2009).CrossRefGoogle ScholarPubMed
Wei, Y., Li, Y., Zhu, L., Liu, Y., Lei, X., Wang, G., Wu, Y., Mi, Z., Liu, J., Wang, H., and Gao, H.: Evading the strength–ductility trade-off dilemma in steel through gradient hierarchical nanotwins. Nat. Commun. 5, 3580 (2014).CrossRefGoogle ScholarPubMed
Li, N., Wang, J., Huang, J., Misra, A., and Zhang, X.: In situ TEM observations of room temperature dislocation climb at interfaces in nanolayered Al/Nb composites. Scr. Mater. 63, 363366 (2010).CrossRefGoogle Scholar
Wang, J., Hoagland, R.G., and Misra, A.: Room-temperature dislocation climb in metallic interfaces. Appl. Phys. Lett. 94, 131910 (2009).CrossRefGoogle Scholar
Liao, X.Z., Srinivasan, S.G., Zhao, Y.H., Baskes, M.I., Zhu, Y.T., Zhou, F., Lavernia, E.J., and Xu, H.F.: Formation mechanism of wide stacking faults in nanocrystalline Al. Appl. Phys. Lett. 84, 35643566 (2004).CrossRefGoogle Scholar
Hattar, K., Misra, A., Dosanjh, M.R.F., Dickerson, P., Robertson, I.M., and Hoagland, R.G.: Direct observation of crack propagation in copper–niobium multilayers. J. Eng. Mater. Technol. 134, 021014 (2012).CrossRefGoogle Scholar
Liu, Z., Monclús, M.A., Yang, L.W., Castillo-Rodríguez, M., Molina-Aldareguía, J.M., and LLorca, J.: Tensile deformation and fracture mechanisms of Cu/Nb nanolaminates studied by in situ TEM mechanical tests. Extreme Mech. Lett. 25, 6065 (2018).CrossRefGoogle Scholar
Li, N., Mara, N.A., Wang, J., Dickerson, P., Huang, J.Y., and Misra, A.: Ex situ and in situ measurements of the shear strength of interfaces in metallic multilayers. Scr. Mater. 67, 479482 (2012).CrossRefGoogle Scholar
Mara, N., Bhattacharyya, D., Dickerson, P., Hoagland, R., and Misra, A.: Deformability of ultrahigh strength 5 nm Cu/Nb nanolayered composites. Appl. Phys. Lett. 92, 1901 (2008).CrossRefGoogle Scholar
Derby, B., Cui, Y., Baldwin, J.K., and Misra, A.: Effects of substrate temperature and deposition rate on the phase separated morphology of co-sputtered, Cu–Mo thin films. Thin Solid Films 647, 5056 (2018).CrossRefGoogle Scholar
Cui, Y., Derby, B., Li, N., and Misra, A.: Design of bicontinuous metallic nanocomposites for high-strength and plasticity. Mater. Des., 166, 107602 (2019).CrossRefGoogle Scholar

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