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A Homemade Vacuum Forceps For Mounting Small SEM Samples

Published online by Cambridge University Press:  14 March 2018

Sol Sepsenwol*
Affiliation:
University of Wisconsin, Stevens Point

Extract

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Very small samples (under 1 mm) prepared for SEM viewing can be sprinkled randomly on an adhesive-coated stub, or manipulated into position with various tools (fine forceps, pointed stick, cotton applicator, hair brush) under a magnifier or stereo microscope. None of these methods allows reliable, damage-free control over the orientation of the sample. Here follow plans for a simple, portable “Vacuum forceps” to create a mild vacuum th rough a micro-fme tip to hold and orient SEM samples as they are applied to the adhesive. It is also useful for sorting samples. Commercial vacuum forceps with on-board vacuum range in price from $500 to $900. This unit was built from new parts for under $100.

The vacuum pump is from a portable motorized pipetter, such as the Drurnmond Scientific Portable Pipet Aid, or Mano stat Mopet (Figure 1). We have used the Drummond 9V motor and pump assembly.

Type
Microscopy 101
Copyright
Copyright © Microscopy Society of America 2004