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Structural and mechanical studies of Fe-Cr thin films deposited by ion-beam sputtering

Published online by Cambridge University Press:  28 January 2005

E. Le Bourhis
Affiliation:
Laboratoire de Métallurgie Physique, UMR 6630 CNRS, Université de Poitiers, bâtiment SP2MI, Téléport 2, boulevard Marie et Pierre Curie, BP 30179, 86962 Futuroscope-Chasseneuil Cedex, France
P. Goudeau*
Affiliation:
Laboratoire de Métallurgie Physique, UMR 6630 CNRS, Université de Poitiers, bâtiment SP2MI, Téléport 2, boulevard Marie et Pierre Curie, BP 30179, 86962 Futuroscope-Chasseneuil Cedex, France
J.-P. Eymery
Affiliation:
Laboratoire de Métallurgie Physique, UMR 6630 CNRS, Université de Poitiers, bâtiment SP2MI, Téléport 2, boulevard Marie et Pierre Curie, BP 30179, 86962 Futuroscope-Chasseneuil Cedex, France
W. Al-Khoury
Affiliation:
Laboratoire de Métallurgie Physique, UMR 6630 CNRS, Université de Poitiers, bâtiment SP2MI, Téléport 2, boulevard Marie et Pierre Curie, BP 30179, 86962 Futuroscope-Chasseneuil Cedex, France Atomic Energy Commission of Syria, PO Box 6091, Damascus, Syria
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Abstract

Fe$_{1-x}$Crx thin films on Si and fused-SiO2 substrates were prepared using ion-beam sputtering deposition. Films with x = 0.69 and x = 0.49 were characterised by X-ray diffraction and conversion electron Mössbauer spectroscopy experiments, and concurrently the elastic and plastic behaviours were investigated through indentation tests. For x = 0.69, the paramagnetic bcc structure is observed, while the indentation modulus and hardness values are found to be 160 and 8.7 GPa, respectively. For x = 0.49, a strongly $\langle 200\rangle$-textured paramagnetic phase is evidenced, having the A15 structure. Mössbauer measurements also allowed the site occupancy to be determined. The structural change from bcc to A15 phase yields a 50% increase in hardness, while the indentation modulus remains unchanged. This particular behaviour is discussed in terms of distances between near neighbours and Burgers vector length in both bcc and A15 structures. The results obtained here provide motivation to pursue the present study through wear experiments.

Keywords

Type
Research Article
Copyright
© EDP Sciences, 2005

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References

Hishinuma, A., Isozaki, S., Takaki, S., Abiko, K., Phys. Status Solidi A 160, 431 (1997) 3.0.CO;2-B>CrossRef
Zabel, H., J. Phys.-Cond. Matter 11, 9303 (1999) CrossRef
Burke, S.K., Cywinski, R., Davis, J.R., Rainford, B.D., J. Phys. F: Met. Phys. 13, 451 (1983) CrossRef
Dubiel, S.M., Inden, G., Z. Metallkd. 78, 544 (1987)
Miller, M.K., Russel, K.F., Surf. Sci. 266, 232 (1992) CrossRef
Gruenberg, P., Schreiber, R., Pang, Y., Brodsky, M.B., Sowers, H., Phys. Rev. Lett. 57, 2442 (1986) CrossRef
Xia, S.K., Baggio-Saitovitch, E., Larica, C., Phys. Rev. B 49, 927 (1994) CrossRef
Sumiyama, K., Ohshima, N., Nakamura, Y., Trans. Jap. Inst. Met. 28, 699 (1987) CrossRef
Duc, N.H., Fnidiki, A., Teillet, J., Ben Youssef, J., Le Gall, H., J. Appl. Phys. 88, 4778 (2000) CrossRef
Levin, A.A., Meyer, D.C., Tselev, A., Gorbunov, A., Pompe, W., Paufler, P., J. Alloy Compd. 334, 159 (2002) CrossRef
Levin, A.A., Meyer, D.C., Gorbunov, A., Tselev, A., Pompe, W., Paufler, P., J. Alloy Compd. 347, 171 (2002) CrossRef
Gorbunov, A., Levin, A.A., Mensch, A., Meyer, D.C., Tselev, A., Paufler, P., Pompe, W., Eckert, D., Appl. Surf. Sci. 197-198, 475 (2002) CrossRef
Levin, A.A., Meyer, D.C., Gorbunov, A., Mensch, A., Pompe, W., Paufler, P., J. Alloy Compd. 360, 107 (2003) CrossRef
Bodin, D., Eymery, J.P., Nucl. Instrum. Methods B 16, 424 (1986) CrossRef
Oliver, W.C., Pharr, G.M., J. Mater. Res. 7, 1564 (1992) CrossRef
Powder Diffraction File of the International Centre for Diffraction Data, PDF-ICDD Card No. 87-0721
Powder Diffraction File of the International Centre for Diffraction Data, PDF-ICDD Card No. 85-1336
Windischmann, H., J. Appl. Phys. 62, 1800 (1987) CrossRef
B.E Warren, X-Ray Diffraction, 1st edn. (Addison-Wesley Pub., Reading, 1969)
Bimbault, L., Badawi, K.F., Goudeau, P., Branger, V., Durand, N., Thin Solid Films 275, 40 (1996) CrossRef
Kimoto, K., Nishida, I., Thin Solid Films 17, 49 (1973) CrossRef
Saraf, L., Wang, C., Engelhard, M.H., Baer, D.R., Appl. Phys. Lett. 82, 2230 (2003) CrossRef
Fisher, S.M., Kaul, S.N., Kronmüller, H., J. Magn. Magn. Mater. 226-230, 540 (2001) CrossRef
Sumiyama, K., Ezawa, H., Nakamura, Y., J. Phys. Chem. Solids 48, 255 (1987) CrossRef
Saha, R., Nix, W.D., Acta Mater. 50, 23 (2002) CrossRef
Mencik, J., Munz, D., Quandt, E., Weppelmann, E.R., Swain, M.V., J. Mater. Res. 12, 2475 (1997) CrossRef
C.J. Smithells, E.A. Brandes, Metals Reference Book, 5th edn. (Butterworth, London, 1976)
P. Goudeau, P.O. Renault, P. Villain, C. Coupeau, V. Pelosin, B. Boubeker, K.F. Badawi, Thin Solid Films 398-399, 496 (2001)
Villain, P., Goudeau, P., Renault, P.-O., Badawi, K.F., Appl. Phys. Lett. 81, 4365 (2002) CrossRef
Yu, D.Y.W., Spaepen, F., J. Appl. Phys. 95, 2991 (2004) CrossRef
Huang, H., Spaepen, S., Acta Mater. 48, 3261 (2000) CrossRef
Batthacharya, A.K., Nix, W.D., Int. J. Solids Struct. 24, 1287 (1988) CrossRef
D. Hull, Introduction to Dislocations, 2nd edn. (Pergamon Press, Oxford, 1981)
Farkas, D., Schon, C.G., De Lima, M.S.F., Goldenstein, H., Acta Mater. 44, 409 (1996) CrossRef
Kelley, M.J., Stoloff, N.S., Metall. Trans. A 7, 331 (1976) CrossRef
Raj, S.V., Mater. Sci. Eng. A 201, 229 (1995) CrossRef
J.G. Swadener, I. Rosales, J.H. Schneibel, Mat. Res. Soc. Symp. Proc. 646, N4.2.1. (2001)
K.L. Johnson, Contact Mechanics, 1st edn. (Cambridge University Press, Cambridge, 1985)
Musil, J., Surf. Coat. Tech. 125, 515 (2000) CrossRef
Badawi, K.F., Villain, P., Goudeau, P., Renault, P.-O., Appl. Phys. Lett. 80, 4705 (2002) CrossRef