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Temperature-Dependent Onset of Yielding in Dislocation-Free Silicon: Evidence of a Brittle-To-Ductile Transition

Published online by Cambridge University Press:  15 February 2011

R. H. Folk II
Affiliation:
Dept. of Materials Science and Eng., University of Pennsylvania, Phila. Pa., 19072
M. Khantha
Affiliation:
Dept. of Materials Science and Eng., University of Pennsylvania, Phila. Pa., 19072
D. P. Pope
Affiliation:
Dept. of Materials Science and Eng., University of Pennsylvania, Phila. Pa., 19072
V. Vitek
Affiliation:
Dept. of Materials Science and Eng., University of Pennsylvania, Phila. Pa., 19072
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Abstract

An investigation of the brittle-to-ductile transition (BDT) in silicon has been conducted on essentially dislocation-free silicon test specimens made by photolithography. No pre-cracks or additional dislocation sources were introduced into the samples. Three-point bending tests of the samples reveals a well defined transition from brittle fracture of the specimens to complete yielding near 732°C at a crosshead displacement rate of 0.1 mm/min. Limited plasticity is observed below 732°C but is insufficient to prevent crack propagation suggesting that yielding is not dislocation mobility limited. Instead the transition may be controlled by the nucleation of a sufficient density of dislocations. Further support comes from the results of experiments conducted at temperatures below 732°C in which samples were rapidly pre-loaded within the linearly elastic regime, then immediately retested. This rapid pre-loading results in a lower transition temperature. This would not be expected if dislocation mobility controlled the BDT. Instead, it is believed that the transition only occurs when a sufficient density of dislocations has nucleated within the sample. In these experiments, the pre-loading event may increase the dislocation nucleation rate. The source of the dislocations in these defect free samples is still under investigation.

Type
Research Article
Copyright
Copyright © Materials Research Society 1999

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References

1. Hirsch, P. B., S., F. R., Roberts, S. G., and Samuels, J., Proc. R. Soc. Lond. A421, pp. 2553 (1989).Google Scholar
2. Brede, M., Acta Metall. Mater. 41, No. 1, pp. 211228 (1993).Google Scholar
3. Nitzsche, V. R. and Hsia, K. J., Mat. Sci. and Eng. A176, pp. 155164 (1994).Google Scholar
4. Pearson, G. L., Read, W. T. Jr., and Feldmann, W. L., Acta Met. 5, pp. 181191 (1957).Google Scholar
5. Brenner, S. S., J. Applied Phy., 27, No. 12, pp. 14841491 (1956).Google Scholar
6. Brenner, S. S., J. Applied Phy., 28, No. 9, pp. 10231026 (1957).Google Scholar
7. Patel, J. R. and Chaudhuri, A. R., J. Applied Phy., 34, No. 9, pp. 27882799 (1963).Google Scholar