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Synthesis of HTCMgFe for the degradation of indigo carmine through heterogeneous photo-Fenton treatment

Published online by Cambridge University Press:  26 November 2020

I. Cosme-Torres ,
M.G. Macedo-Miranda ,
S.M. Martinez-Gallegos ,
J.C. González-Juárez ,
G. Roa-Morales ,
F.J. Illescas-Martínez  and
J. Jimenez-Becerril
I. Cosme-Torres
Affiliation:
Tecnológico Nacional de México/Instituto Tecnológico de Toluca, Av. Tecnológico s/n, Colonia Agrícola Bellavista, C.P. 52149, Metepec, México.
M.G. Macedo-Miranda*
Affiliation:
Tecnológico Nacional de México/Instituto Tecnológico de Toluca, Av. Tecnológico s/n, Colonia Agrícola Bellavista, C.P. 52149, Metepec, México.
S.M. Martinez-Gallegos
Affiliation:
Tecnológico Nacional de México/Instituto Tecnológico de Toluca, Av. Tecnológico s/n, Colonia Agrícola Bellavista, C.P. 52149, Metepec, México.
J.C. González-Juárez
Affiliation:
Tecnológico Nacional de México/Instituto Tecnológico de Toluca, Av. Tecnológico s/n, Colonia Agrícola Bellavista, C.P. 52149, Metepec, México.
G. Roa-Morales
Affiliation:
Universidad Autónoma del Estado de México, Facultad de Química, Paseo Colón intersección Paseo Tollocan s/n, C.P. 50120, Toluca, México
F.J. Illescas-Martínez
Affiliation:
Tecnológico Nacional de México/Instituto Tecnológico de Toluca, Av. Tecnológico s/n, Colonia Agrícola Bellavista, C.P. 52149, Metepec, México.
J. Jimenez-Becerril
Affiliation:
Instituto Nacional de Investigaciones Nucleares, Carretera México-Toluca s/n, La Marquesa, C.P. 52750, Ocoyoacac México.
*
mmacedom@toluca.tecnm.mx
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Abstract

The heterogeneous catalyst HTCMgFe was used in the degradation of the IC, through the heterogeneous photo-fenton treatment, this material in combination with H2O2 and UV light degraded the dye in 30 min at pH 3. As the amount of HTCMgFe increases the degradation it was accelerated because there are more active catalytic sites of Fe2+ on the surface of the material, which generates a greater amount of •OH radicals. The HTCMgFe was characterized by infrared spectroscopy (FTIR), scanning electron microscopy (SEM) and X-ray energy dispersive elemental analysis (EDS). The UV-vis spectrum shows that the absorption bands belonging to the chromophore group of the IC disappear as the treatment time passes, indicating the degradation of the dye.

Type
Articles
Information
MRS Advances , Volume 5 , Issue 62: International Materials Research Congress XXIX , 2020 , pp. 3273 - 3282
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Copyright
Copyright © The Author(s), 2020, published on behalf of Materials Research Society by Cambridge University Press

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