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Combining Fast Imaging and Variable Temperature Studies in Atomic Force Microscopy

Published online by Cambridge University Press:  28 May 2018

Sergei Magonov  and
Shijie Wu
Sergei Magonov*
Affiliation:
SPM Labs LLC, Tempe AZ85283USA
Shijie Wu
Affiliation:
Keysight Technologies, Santa Clara, CA95051USA
*
*(Email: magonov@spmlabs.com)
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Abstract

Fast imaging in Atomic Force Microscopy enhances the capability of studying phase transitions and surface properties of materials at variable temperatures. This is demonstrated by measurements of several polymers [poly(diethylsiloxane), low-density polyethylene and ethylene-octene copolymer] and bitumen at low (down to -20°C) and high (up to +150°C) temperatures. Monitoring of structural transitions was performed at small and large (up to 40 μm) areas with 1-5°C/min cooling/heating rates. Novel data about dynamics and structural transitions of mesomorphic transitions and crystallization were obtained.

Keywords

crystallizationscanning probe microscopy (SPM)polymer
Type
Articles
Information
MRS Advances , Volume 3 , Issue 44: Characterization, Modeling and Theory , 2018 , pp. 2705 - 2712
Copyright
Copyright © Materials Research Society 2018 

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