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Application of ζ-factor Microanalysis to Measure Phase Compositions in Ultrahard Ceramics and Complex Concentrated Alloys

Published online by Cambridge University Press:  30 July 2021

Christopher Marvel
Affiliation:
Lehigh University, Bethlehem, Pennsylvania, United States
Joshua Smeltzer
Affiliation:
Lehigh University, United States
Kristopher Behler
Affiliation:
Army Research Laboratory, United States
B. Chad Hornbuckle
Affiliation:
Army Research Laboratory, United States
Jerry LaSalvia
Affiliation:
Army Research Laboratory, United States
Kristopher Darling
Affiliation:
Army Research Laboratory, United States
Masashi Watanabe
Affiliation:
Lehigh University, Bethlehem, Pennsylvania, United States
Martin Harmer
Affiliation:
Lehigh University, United States
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Abstract

Image of the first page of this content. For PDF version, please use the ‘Save PDF’ preceeding this image.'
Type
Many Detectors Make Lights Work: Advances in Microanalysis of Light Elements in Synthetic and Natural Materials
Copyright
Copyright © The Author(s), 2021. Published by Cambridge University Press on behalf of the Microscopy Society of America

References

Watanabe, M. and Williams, D. B.. "The quantitative analysis of thin specimens: a review of progress from the Cliff-Lorimer to the new ζ-factor methods." Journal of microscopy 221, no. 2 (2006): 89-109.10.1111/j.1365-2818.2006.01549.xCrossRefGoogle ScholarPubMed
Marvel, C.J., Behler, K. D., LaSalvia, J. C., Domnich, V., Haber, R. A., Watanabe, M., and Harmer, M. P.. "Extending ζ-factor microanalysis to boron-rich ceramics: Quantification of bulk stoichiometry and grain boundary composition." Ultramicroscopy 202 (2019): 163-172.10.1016/j.ultramic.2019.04.008CrossRefGoogle ScholarPubMed
Smeltzer, J.A., Marvel, C.J., Hornbuckle, B.C., Roberts, A.J., Marsico, J.M., Giri, A.K., Darling, K.A., Rickman, J.M., Chan, H.M., and Harmer, M.P.. "Achieving ultrahard refractory multi-principal element alloys via mechanical alloying." Materials Science and Engineering: A 763 (2019): 138140.10.1016/j.msea.2019.138140CrossRefGoogle Scholar
Behler, K.D., Marvel, C.J., LaSalvia, J.C., Walck, S.D., Harmer, M.P.. “Observations of grain boundary chemistry variations in a boron carbide processed with oxide additives.Scripta 142 Materialia (2018): 106-10.10.1016/j.scriptamat.2017.08.033CrossRefGoogle Scholar
Kuwelkar, K.A.. “Chemical and structural characterization of boron carbide powders and ceramics.” Dissertation, Rutgers University (2016).Google Scholar
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Application of ζ-factor Microanalysis to Measure Phase Compositions in Ultrahard Ceramics and Complex Concentrated Alloys
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