Hostname: page-component-8448b6f56d-42gr6 Total loading time: 0 Render date: 2024-04-22T13:39:31.231Z Has data issue: false hasContentIssue false

4D-STEM analysis of an amorphous-crystalline polymer blend: combined nanocrystalline and RDF mapping.

Published online by Cambridge University Press:  30 July 2021

Jennifer Donohue
Affiliation:
University of California, Berkeley, United States
Karen C Bustillo
Affiliation:
Lawrence Berkeley National Laboratory, United States
Steven E Zeltmann
Affiliation:
University of California, Berkeley, United States
Colin Ophus
Affiliation:
Lawrence Berkeley National Laboratory, California, United States
Benjamin Savitzky
Affiliation:
Lawrence Berkeley National Laboratory, California, United States
Mary Ann Jones
Affiliation:
DOW Chemical Company, United States
Gregory F Meyers
Affiliation:
DOW Chemical Company, United States
Andrew Minor
Affiliation:
UC Berkeley, Berkeley, California, United States

Abstract

Image of the first page of this content. For PDF version, please use the ‘Save PDF’ preceeding this image.'
Type
Diffraction Imaging Across Disciplines
Copyright
Copyright © The Author(s), 2021. Published by Cambridge University Press on behalf of the Microscopy Society of America

References

Panova, O., Ophus, C., Takacs, C. J., Bustillo, K. C., Balhorn, L., Salleo, A., … & Minor, A. M. (2019). Diffraction imaging of nanocrystalline structures in organic semiconductor molecular thin films. Nature materials, 1.Google Scholar
Mu, X., Mazilkin, A., Sprau, C., Colsmann, A., & Kübel, C. (2019). Mapping structure and morphology of amorphous organic thin films by 4D-STEM pair distribution function analysis. Microscopy.Google ScholarPubMed
Ophus, C. (2019). Four-Dimensional Scanning Transmission Electron Microscopy (4D-STEM): From Scanning Nanodiffraction to Ptychography and Beyond. Microscopy and Microanalysis, 25(3), 563-582.Google ScholarPubMed
Narten, A. H. (1989). Radial distribution of carbon atoms in crystalline and molten polyethylene from x-ray diffraction. The Journal of chemical physics, 90(10), 5857-5860.CrossRefGoogle Scholar
Wang, C. S., & Yeh, G. S. Y. (1981). Effects of Radiation on the Structure of Polypropylene. Polymer Journal, 13(8), 741-747.Google Scholar
Curro, J. G., Weinhold, J. D., Rajasekaran, J. J., Habenschuss, A., Londono, J. D., & Honeycutt, J. D. (1997). Intermolecular packing in stereoregular polypropylene liquids: Comparison between theory and X-ray scattering experiments. Macromolecules, 30(20), 6264-6273.Google Scholar
Marigo, A., Martorana, A., Marega, C., & Zannetti, R. (1987). Radial atomic distribution function and structure models of isotactic polypropylene. Die Makromolekulare Chemie, Rapid Communications, 8(1), 23-26.Google Scholar