Hostname: page-component-76fb5796d-22dnz Total loading time: 0 Render date: 2024-04-25T07:09:48.228Z Has data issue: false hasContentIssue false

Response of fusion plasma-facing materials to nanosecond pulses of extreme ultraviolet radiation

Published online by Cambridge University Press:  31 August 2018

Jaroslav Straus
Affiliation:
Institute of Plasma Physics of the Czech Academy of Sciences, Za Slovankou 1782/3, 182 00 Prague 8, Czech Republic
Karel Kolacek*
Affiliation:
Institute of Plasma Physics of the Czech Academy of Sciences, Za Slovankou 1782/3, 182 00 Prague 8, Czech Republic
Jiri Schmidt
Affiliation:
Institute of Plasma Physics of the Czech Academy of Sciences, Za Slovankou 1782/3, 182 00 Prague 8, Czech Republic
Oleksandr Frolov
Affiliation:
Institute of Plasma Physics of the Czech Academy of Sciences, Za Slovankou 1782/3, 182 00 Prague 8, Czech Republic
Monika Vilemova
Affiliation:
Institute of Plasma Physics of the Czech Academy of Sciences, Za Slovankou 1782/3, 182 00 Prague 8, Czech Republic
Jiri Matejicek
Affiliation:
Institute of Plasma Physics of the Czech Academy of Sciences, Za Slovankou 1782/3, 182 00 Prague 8, Czech Republic
Ales Jager
Affiliation:
Institute of Physics of the Czech Academy of Sciences, Na Slovance 1999/2, 182 21 Prague 8, Czech Republic
Libor Juha
Affiliation:
Institute of Plasma Physics of the Czech Academy of Sciences, Za Slovankou 1782/3, 182 00 Prague 8, Czech Republic Institute of Physics of the Czech Academy of Sciences, Na Slovance 1999/2, 182 21 Prague 8, Czech Republic
Martina Toufarova
Affiliation:
Institute of Physics of the Czech Academy of Sciences, Na Slovance 1999/2, 182 21 Prague 8, Czech Republic
Andrey Choukourov
Affiliation:
Institute of Physics of the Czech Academy of Sciences, Na Slovance 1999/2, 182 21 Prague 8, Czech Republic Faculty of Mathematics and Physics, Charles University in Prague, Ke Karlovu 3, 121 16 Prague 2, Czech Republic
Koichi Kasuya
Affiliation:
Institute of Applied Flow, 3-24-4 Utsukushigaoka-Nishi, Aoba, Yokohama, Kanagawa 225-0001, Japan
*
Author for correspondence: Karel Kolacek, Institute of Plasma Physics CAS, Za Slovankou 1782/3, 182 00 Prague 8, Czech Republic. E-mail: kolacek@ipp.cas.cz

Abstract

The experimental study of damage to tungsten (W), molybdenum (Mo), and silicon carbide (SiC) surfaces induced by focused extreme ultraviolet laser radiation (λ ~ 47 nm/~1.5 ns/21–40 µJ) is presented. It was found that W and Mo behaved similarly: during the first shot, the damaged area is covered by melted and re-solidified material, in which circular holes appear – residua of just opened pores/bubbles, from which pressurized gas/vapors escaped. Next cracks and ruptures appear and the W has a tendency to delaminate its surface layer. Contrary, single-crystalline SiC has negligible porosity and sublimates; therefore, no escape of “pressurized” gas and no accompanying effects take place. Moreover, SiC at sublimating temperature decomposes to elements; therefore, the smooth crater morphology can be related to local laser energy density above ablation threshold. When more shots are accumulated, in all three investigated materials, the crater depth increases non-linearly with number of these shots. The surface morphology was investigated by an atomic force microscope, the surface structure was imaged by a scanning electron microscope (SEM), and the structure below the surface was visualized by SEM directed into a trench that is milled by focused ion beam. Additionally, structural changes in SiC were revealed by Raman spectroscopy.

Type
Research Article
Copyright
Copyright © Cambridge University Press 2018 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

A 2013–2020 roadmap towards Inertial Fusion Energy based on a 2007–2012 watching brief. Available at http://web.luli.polytechnique.fr/IFE-KiT/docs/IFE_roadmap_Europe.pdfGoogle Scholar
Alvarez, J, Garoz, D, Gonzalez-Arrabal, R, Rivera, A and Perlado, M (2011) The role of spatial and temporal radiation deposition in inertial fusion chambers: the case of HiPER. Nuclear Fusion 51, 053019.Google Scholar
Blanchard, JP and Martin, CJ (2005) Thermomechanical effects in a laser IFE first wall. Journal of Nuclear Materials 347, 192206.Google Scholar
Blejchar, T, Nevrlý, V, Vasinek, M, Dostal, M, Kozubkova, M, Dlabka, J, Stachoň, M, Juha, L, Bitala, P, Zelinger, Z, Pira, P and Wild, J (2016) Desorption/ablation of lithium fluoride induced by extreme ultraviolet laser radiation. Nukleonika 61, 131138.Google Scholar
Buratin, S, Bashtova, K and Kong, MC (2017) Thermal effects on 3D crater shape during IR laser ablation of monocrystalline silicon: from femtoseconds to microseconds. Journal of Applied Physics 122, 023105.Google Scholar
Caro, A (2009) “LIFE Materials: Topical Assessment Report for LIFE Volume 1 TOPIC: Solid First Wall and Structural Components TASK: Radiation Effects on First Wall”, Technical report of LLNL, No. 35. Available at http://dx.doi.org/10.2172/945884Google Scholar
Chalupsky, J, Juha, L, Kuba, J, Cihelka, J, Hajkova, V, Koptyaev, S, Krasa, J, Velihan, A, Bergh, M, Caleman, C, Hajdu, J, Bionta, RM, Chapman, H, Hau-Riege, SP, London, RA, Jurek, M, Krzywinski, J, Nietubyc, R, Pelka, JB, Sobierajski, R, Meyer-ter-Vehn, J, Tronnier, A, Sokolowski-Tinten, K, Stojanowic, N, Tiedtke, K, Toleikis, S, Tschentscher, T, Wabnitz, H and Zastrau, U (2007) Characteristics of focused soft X-ray free-electron laser beam determined by ablation of organic molecular solids. Optics Express 15, 60366043.Google Scholar
Chalupsky, J, Juha, L, Hajkova, V, Cihelka, J, Vyšín, L, Gautier, J, Hajdu, J, Hau-Riege, SP, Jurek, M, Krzywinski, J, London, RA, Papalazarou, E, Pelka, JB, Rey, G, Sebban, S, Sobierajski, R, Stojanovic, N, Tiedtke, K, Toleikis, S, Tschentscher, T, Valentin, C, Wabnitz, H and Zeitoun, P (2009) Non-thermal desorption/ablation of molecular solids induced by ultra-short soft X-ray pulses. Optics Express 17, 208217.Google Scholar
Cheung, R (ed.) (2006) Silicon Carbide Microelectromechanical Systems for Harsh Environments. London: Imperial College Press, p. 3.Google Scholar
Craxton, RS, Anderson, KS, Boehly, TR, Goncharov, VN, Harding, DR, Knauer, JP, McCrory, RL, McKenty, PW, Meyerhofer, DD, Myatt, JF, Schmitt, AJ, Sethian, JD, Short, RW, Skupsky, S, Theobald, W, Kruer, WL, Tanaka, K, Betti, R, Collins, TJB, Delettrez, JA, Hu, SX, Marozas, JA, Maximov, AV, Michel, DT, Radha, PB, Regan, SP, Sangster, TC, Seka, W, Solodov, AA, Soures, JM, Stoeckl, C and Zuegel, JD (2015) Direct-drive inertial confinement fusion: a review. Physics of Plasmas 22, 110501.Google Scholar
Garoz, D, Páramo, AR, Rivera, A, Perlado, JM and González-Arrabal, R (2016) Modelling the thermomechanical behaviour of the tungsten first wall in HiPER laser fusion scenarios. Nuclear Fusion 56, 126014.Google Scholar
Gemini, L, Margarone, D, Trusso, S, Juha, L, Limpouch, J, Mocek, T and Ossi, PM (2013) Generation of periodic structures on SiC upon laser plasma XUV/NIR radiations. Laser and Particle Beams 31, 547550.Google Scholar
Hassanein, A and Morozov, V (2004) Development of comprehensive and integrated models for inertial fusion cavity dynamics, Argonne National Laboratory, Energy Technology Division, Report ANL-ET/02-04. Available at https://engineering.purdue.edu/CMUXE/Publications/AHR/R02-ANL-ET-02-04.pdfGoogle Scholar
Henke, BL, Gullikson, EM and Davis, JC (1993) X-ray interactions: photoabsorption, scattering, transmission, and reflection at E = 50-30000 eV, Z = 1-92. Atomic Data and Nuclear Data Tables 54, 181342.Google Scholar
Hinoki, T, Snead, LL and Blue, CA (2005) Development of refractory armored silicon carbide by infrared transient liquid phase processing. Journal of Nuclear Materials 347, 207216.Google Scholar
Inertial Fusion Energy Watching Brief 2007–2013. Available at http://web.luli.polytechnique.fr/IFE-KiT/docs/IFE-Watching_brief-FP7.pdfGoogle Scholar
Inogamov, NA, Zhakhovsky, VV, Ashitkov, SI, Emirov, YN, Faenov, AY, Petrov, YV, Khokhlov, VA, Ishino, M, Demaske, BJ, Tanaka, M, Hasegawa, N, Nishikino, M, Tamotsu, S, Pikuz, TA, Skobelev, IY, Ohba, T, Kaihori, T, Ochi, Y, Imazono, T, Fukuda, Y, Kando, M, Kato, Y, Kawachi, T, Anisimov, SI, Agranat, MB, Oleynik, II and Fortov, VE (2015) Surface nanodeformations caused by ultrashort laser pulse. Engineering Failure Analysis 47, 328337.Google Scholar
Jaeglé, P, Sebban, S, Carillon, A, Jamelot, G, Klisnik, A, Zeitoun, P, Rus, B, Nantel, M, Albert, F and Ros, D (1997) Ultraviolet luminescence of CsI and CsCl excited by soft x-ray laser. Journal of Applied Physics 81, 24062409.Google Scholar
Kabeer, FC, Zijlstra, ES and Garcia, ME (2014) Road of warm dense noble metals to the plasma state: ab initio theory of the ultrafast structural dynamics in warm dense matter. Physical Review B 89, 100301(R) 1–5.Google Scholar
Knaster, J, Arbeiter, F, Cara, P, Favuzza, P, Furukawa, T, Groeschel, F, Heidinger, R, Ibarra, A, Matsumoto, H, Mosnier, A, Serizawa, H, Sugimoto, M, Suzuki, H and Wakai, E (2013) IFMIF: overview of the validation activities. Nuclear Fusion 53, 116001.Google Scholar
Kolacek, K, Straus, J, Schmidt, J, Frolov, O, Prukner, V, Shukurov, A, Holy, V, Sobota, J and Fort, T (2012) Nano-structuring of solid surface by extreme ultraviolet Ar8 + laser. Laser and Particle Beams 30, 5763.Google Scholar
Kolacek, K, Schmidt, J, Straus, J and Frolov, O (2015 a) Calibration of windowless photodiode for extreme ultraviolet pulse energy measurement. Applied Optics 54, 1045410459.Google Scholar
Kolacek, K, Schmidt, J, Straus, J, Frolov, O, Juha, L and Chalupsky, J (2015 b) Interaction of extreme ultraviolet laser radiation with solid surface: ablation, desorption, nanostructuring, 20th International Symposium on High Power Laser System and Applications, 25–29. 08.2014, Chengdu, China, Proceeding of SPIE 9255, 92553U-1 to 9. Eds. Ch. Tang, S. Chen, X. Tang.Google Scholar
Krstic, PS, Allain, JP, Dominguez-Gutierrez, FJ and Bedoya, F (2018) Unraveling the surface chemistry processes in lithiated and boronized plasma material interfaces under extreme conditions. Matter and Radiation at Extremes 3, 165187.Google Scholar
Krzywinski, J, Andrejczuk, A, Bionta, RM, Burian, T, Chalupský, J, Jurek, M, Kirm, M, Nagirnyi, V, Sobierajski, R, Tiedtke, K, Vielhauer, S and Juha, L (2017) Saturation of a Ce:Y3Al5O12 scintillator response to ultra-short pulses of extreme ultraviolet, soft X-ray and X-ray laser radiation. Optical Materials Express 7, 665675.Google Scholar
Latkowski, JF, Abbott, RP, Schmitt, RC and Bell, BK (2005) Effect of multi-shot X-ray exposures in IFE armor materials. Journal of Nuclear Materials 347, 255265.Google Scholar
Le Pape, S, Zeitoun, P, Idir, M, Dhez, P, Rocca, JJ and Francois, M (2002) Electromagnetic-field distribution measurements in the soft X-ray range: full characterization of the soft X-ray laser beam. Physical Review Letters 88, 183901.Google Scholar
Medvedev, N, Li, Z and Ziaja, B (2015) Thermal and non-thermal melting of silicon under femtosecond X-ray irradiation. Physical Review B 91, 054113.Google Scholar
Najmabadi, F, Pulsifer, J and Tillack, M (2006) Update on armor simulation experiments at Dragonfire facility, Proceedings of 15th High Average Power Laser Workshop, General Atomics, San Diego, CA, August 8–9, 2006.Google Scholar
Nakashima, S and Harima, H (1997) Raman investigation of SiC polytypes. Physica Status Solidi A – Applied Research 162, 3964, Table 2, p. 46.Google Scholar
National Research Council (2013) Chapter 4. In Ahearne, JF (ed.), Assessment of Inertial Confinement Fusion Targets. Washington, DC: The National Academies Press, pp. 4586. http://dx.doi.org/10.17226/18288Google Scholar
Neilson, G (2014) Chapter 18. In Neilson, G (ed.), Magnetic Fusion Energy: From Experiments to Power Plants, 1st edn. Amsterdam, Boston, Cambridge, Heidelberg, London, New York, Oxford, Paris, San Diego, San Francisco, Singapore, Sydney, Tokyo: Woodhead Publishing, pp. 549575.Google Scholar
Perlado, JM, Dominguez, E, Lodi, D, Malerba, L, Marian, J, Prieto, J, Salvador, M, de la Rubia, TD, Alonso, E, Caturla, MJ and Colombo, L (2001) Multiscale modeling of radiation damage of metals and SiC in inertial fusion reactors. Fusion Technology 39, 579584.Google Scholar
Pikuz, T, Faenov, A, Matsuoka, T, Matsuyama, S, Yamauchi, K, Ozaki, N, Albertazzi, B, Inubushi, Y, Yabashi, M, Tono, K, Sato, Y, Yumoto, H, Ohashi, H, Pikuz, S, Grum-Grzhimailo, AN, Nishikino, M, Kawachi, T, Ishikawa, T and Kodama, R (2015) 3D visualization of XFEL beam focusing properties using LiF crystal X-ray detector. Scientific Reports 5, 17713.Google Scholar
Raffray, AR, El-Guebaly, LA, Federici, G, Haynes, D, Najmabadi, F and Petti, D and the ARIES-IFE Team (2004) Dry-wall survival under IFE conditions, Fusion Science & Technology 46, 417437.Google Scholar
Renk, TJ, Provencio, PP, Tanaka, TJ, Olson, CL, Peterson, RR, Stolp, JE, Schroen, DG and Knowles, TR (2005) Chamber wall materials response to pulsed ions at power-plant level fluences. Journal of Nuclear Materials 347, 266288.Google Scholar
Romashevskiy, SA, Ashitkov, SI and Agranat, MB (2016) Surface microcavities at nanoscale depths produced by ultrafast laser pulses. Applied Physics Letters 109, 261601.Google Scholar
Ryutov, DD (2003) Thermal stresses in the reflective X-ray optics for the Linac Coherent Light Source. Review of Scientific Instruments 74, 37223725.Google Scholar
Sawan, ME, Ghoniem, NM, Snead, L and Katoh, Y (2011) Damage production and accumulation in SiC structures in inertial and magnetic fusion systems. Journal of Nuclear Materials 417, 445450.Google Scholar
Schmidt, J, Kolacek, K, Straus, J, Prukner, V, Frolov, O and Bohacek, V (2005) Soft X-ray emission of a fast-capillary-discharge device. Plasma Devices and Operations 13, 105109.Google Scholar
Schneider, M, Gunther, CM, Pfau, B, Capotondi, F, Manfredda, M, Zangrando, M, Mahne, N, Raimondi, L, Pedersoli, E, Naumenko, D and Eisebitt, S (2018) In situ single-shot diffractive fluence mapping for X-ray free electron laser pulses. Nature Communications 9, 214.Google Scholar
Schropp, A, Hoppe, R, Meier, V, Patommel, J, Seiboth, F, Lee, HJ, Nagler, B, Galtier, EC, Arnold, B, Zastrau, U, Hastings, JB, Nilsson, D, Uhlen, F, Vogt, U, Hertz, HM and Schroer, CG (2013) Full spatial characterization of a nanofocused X-ray free electron laser beam by ptychographic imaging. Scientific Reports 3, 1633.Google Scholar
Sethian, JD, Colombant, DG, Giuliani, JL, Lehmberg, RH, Myers, MC, Obenschain, SP, Schmitt, AJ, Weaver, J, Wolford, MF, Hegeler, F, Friedman, M, Robson, AE, Bayramian, A, Caird, J, Ebbers, C, Latkowski, J, Hogan, W, Meier, WR, Perkins, LJ, Schaffers, K, Kahlik, SA, Schoonover, K, Sadowski, D, Boehm, K, Carlson, L, Pulsifer, J, Najmabadi, F, Raffray, AR, Tillack, MS, Kulcinski, G, Blanchard, JP, Heltemes, T, Ibrahim, A, Marriott, E, Moses, G, Radell, R, Sawan, M, Santarius, J, Sviatoslavsky, G, Zenobia, S, Ghoniem, NM, Sharafat, S, El-Awady, J, Hu, Q, Duty, C, Leonard, K, Romanoski, G, Snead, LL, Zinkle, SJ, Gentile, C, Parsells, W, Prinksi, C, Kozub, T, Dodson, T, Rose, DV, Renk, T, Olson, C, Alexander, N, Bozek, A, Flint, G, Goodin, DT, Hund, J, Paguio, R, Petzoldt, RW, Schroen, DG, Sheliak, J, Bernat, T, Bittner, D, Karnes, J, Petta, N, Streit, J, Geller, D, Hoffer, JK, McGeoch, MW, Glidden, SC, Sanders, H, Weidenheimer, D, Morton, D, Smith, ID, Bobecia, M, Harding, D, Lehecka, T, Gilliam, SB, Gidcumb, SM, Forsythe, D, Parikh, NR, O'Dell, S and Gorensek, M (2010) The science and technologies for fusion energy with lasers and direct-drive targets. IEEE Transactions on Plasma Science 38, 690703.Google Scholar
Siklitsky, V (1998–2001) Ioffe Physico-Technical Institute Electronic archive (1998–2001) New Semiconductor Materials. Characteristics and Properties. Available at http://www.ioffe.ru/SVA/NSM/Semicond/SiC/thermal.htmlGoogle Scholar
Snead, LL, Nozawa, T, Ferraris, M, Katoh, Y, Shinavski, R and Sawan, M (2011) Silicon carbide composites as fusion power reactor structural materials. Journal of Nuclear Materials 417, 330339.Google Scholar
Sorieul, S, Costantini, J-M, Gosmain, L, Thomé, L and Grob, J-J (2006) Raman spectroscopy of heavy-ion-irradiated α-SiC. Journal of Physics: Condensed Matter 18, 52355251.Google Scholar
Stork, D, Agostini, P, Boutard, J-L, Buckthorpe, D, Diegele, E, Dudarev, SL, English, C, Federici, G, Gilbert, MR, Gonzalez, S, Ibarra, A, Linsmeier, C, Puma, ALMarbach, G, Packer, LW, Raj, B, Rieth, M, Tran, MQ, Ward, DJ and Zinkle, SJ (2014) Materials R&D for a timely DEMO: key findings and recommendations of the EU Roadmap Materials Assessment Group. Fusion Engineering and Design 89, 15861594.Google Scholar
Tanaka, TJ, Rochau, GA, Peterson, RR and Olson, CL (2005) Testing IFE materials on Z. Journal of Nuclear Materials 347, 244254.Google Scholar
Vilemova, M, Pala, Z, Jager, A, Matejicek, J, Chernyshova, M, Kowalska-Strzeciwilk, E, Tonarova, D and Gribkov, VA (2016) Evaluation of surface, microstructure and phase modifications on various tungsten grades induced by pulsed plasma loading. Physica Scripta 91, 034003 (12pp).Google Scholar
von der Linde, D and Sokolowski-Tinten, K (2000) The physical mechanisms of short-pulse laser ablation. Applied Surface Science 154–155, 110.Google Scholar
Wesson, J (2011) Tokamaks 4th edition International Series of Monographs on Physics 149, Oxford Science Publications, Oxford University Press, ISBN 978-0-19-959223-4, Chap. 9.7 Wall conditioning.Google Scholar
Xu, Y, Wang, R, Ma, S, Zhou, L, Shen, YR and Tian, C (2018) Theoretical analysis and simulation of pulsed laser heating at interface. Journal of Applied Physics 123, 025301.Google Scholar
Zhakhovskii, V, Inogamov, N and Nishihara, K (2008) Laser ablation and spallation of crystalline aluminium simulated by Molecular Dynamics, The 5th International Conference on Inertial Fusion Sciences and Applications (IFSA2007), IOP Publishing, Journal of Physics: Conference Series 112, 042080.Google Scholar
Supplementary material: File

Straus et al. supplementary material

Straus et al. supplementary material 1

Download Straus et al. supplementary material(File)
File 2.3 MB