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Preparation and Characterization of L-Aspartic Acid-Intercalated Layered Double Hydroxide

Published online by Cambridge University Press:  01 January 2024

Qi Yuan
Affiliation:
Key Laboratory of Science and Technology of Controllable Chemical Reactions, Ministry of Education, Beijing University of Chemical Technology, Beijing 100029, PR China
Min Wei
Affiliation:
Key Laboratory of Science and Technology of Controllable Chemical Reactions, Ministry of Education, Beijing University of Chemical Technology, Beijing 100029, PR China
Zhiqiang Wang
Affiliation:
Department of Chemistry, Tsinghua University, Beijing 100084, PR China
Ge Wang
Affiliation:
Key Laboratory of Science and Technology of Controllable Chemical Reactions, Ministry of Education, Beijing University of Chemical Technology, Beijing 100029, PR China
Xue Duan*
Affiliation:
Key Laboratory of Science and Technology of Controllable Chemical Reactions, Ministry of Education, Beijing University of Chemical Technology, Beijing 100029, PR China
*
*E-mail address of corresponding author: duanx@mail.buct.edu.cn

Abstract

L-aspartic acid was intercalated into layered double hydroxides by coprecipitation. Two types of well crystallized material were obtained and were characterized by powder X-ray diffraction, Fourier transform infrared spectroscopy, thermogravimetry, differential thermal analysis and polarimetry. Schematic models of two intercalation structures with different basal spacings are given. It is proved that the optical activity of L-aspartic acid is retained during and after the intercalation process.

Type
Research Article
Copyright
Copyright © 2004, The Clay Minerals Society

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