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121Sb MöSsbauer Studies of Graphite–SbF5 Intercalation Compounds
D. H. Mcdaniel, P. Boolchand, W. J. Bresser, P. C. Eklund
Journal: MRS Online Proceedings Library Archive / Volume 20 / 1982
Published online by Cambridge University Press: 15 February 2011, 377
Print publication: 1982
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Stage 2 samples of graphite-SbF5 intercalVtion compounds were prepared by reacting SbF5 with HOPG at 200°C for 5 days. 121Sb Mössbauer spectra taken at 4.2K reveal an intense and narrow feature in the Sb(5+) region and a weak and broad feature in the Sb(3+) region. Interpretation of these data in terms of possible Sb(5+) and Sb(3+) intercalant species is discussed in connection with chemical aspects of intercalation.