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Permalloy particles were fabricated by pulsed excimer laser ablation in distilled water and Tween 80 aqueous solution with the same laser parameters. Nearly spherical particles and irregular and porous fragments were obtained in water due to rapid condensation and growth of the laser ablated clusters. The products obtained in Tween 80 aqueous solution contained well-shaped spheres but some were laser sintered together via laser-particle interactions. Holes or pits were observed on the surface of some particles, which we consider were caused by laser induced bubbles in the liquid. Our results demonstrate the rich environment ablation in liquids can be for novel particle formation.