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X-ray powder diffraction data for a DACH Pt dibromide, cis-[dibromo(1R,2R)-1,2-diaminocyclohexane-κN, κN′] platinum(II)

  • J. Maixner (a1), R. Pažout (a1), I. Nováková (a2), J. Holakovská (a2) and P. Kačer (a2)...

Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for a novel platinum-based anticancer complex cis-[dibromo(1R,2R)-1, 2-diaminocyclohexane-κN, κN′]platinum(II), cis-Pt(C6H14N2)Br2, are presented [a = 11.862(4) Å, b = 7.222(3) Å, c = 13.353(2) Å, β = 97.813(7)°, cell volume V = 1133,36 Å3, Z = 4, space group P21]. All measured lines were indexed and are consistent with the P21 space group. No detectable impurities were observed.

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a)Author to whom correspondence should be addressed. Electronic mail: jaroslav.maixner@vscht.cz

References

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Lock, C. J. L. and Pilon, P. (1981). “Tris[cis-dichloro(1,2-diaminocyclohexane)platinum(II) Hydrate and [cis-dibromo(1,2-diaminocyclohexane)platinum(II),” Acta Crystallogr. B 37, 4549.
Boultif, A. and Louër, D. (2004). “Powder pattern indexing with the dichotomy method,” J. Appl. Crystallogr. 37, 724731.
Smith, G. S. and Snyder, R. L. (1979). “FN: a criterion for rating poder diffraction patterns and evaluating the reliability of powder indexing,” J. Appl. Crystallogr. 12, 6065.
de Wolff, P. M. (1968). “A simplified criterion for the reliability of a powder pattern,” J. Appl. Crystallogr. 1, 108113.

Keywords

X-ray powder diffraction data for a DACH Pt dibromide, cis-[dibromo(1R,2R)-1,2-diaminocyclohexane-κN, κN′] platinum(II)

  • J. Maixner (a1), R. Pažout (a1), I. Nováková (a2), J. Holakovská (a2) and P. Kačer (a2)...

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