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X-ray diffraction data of C16H14O4Ru2M (M=Ge,Si)

  • Yu PuLan (a1), Ding Shuang (a1), Qiao YuanYuan (a1), Yao XinKan (a1), Liu Chong (a1) and Lin ShaoFan (a1)...

Abstract

Two compounds have been studied by means of powder diffraction and their unit cell parameters are reported. The monoclinic cell parameters for dimethylgermanyl-bridged bis cyclopentadienyl tetracarbonyl diruthenium are a=11.03(2) Å, b=13.65(2) Å, c=11.609(2) Å, β=105.81(1)°, Z=4, space group P21/n (No. 14), Dx=2.135 mg/m3. The monoclinic cell parameters for λ-dimethylsilyl-dicyclopentadienyl-π, π′-tetracarbonyl diruthenium, are a=11.113(3) Å, b=13.60(1) Å, c=11.674(7) Å, and β=106.00(3)°, Z=4, space group P21/n (No. 14), and Dx=1.946 mg/m3. The cells found for the two compounds are in good agreement with those obtained from single crystal X-ray diffractometry.

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Xinkan, Yao, Proceedings of Seventh National Conference on X-ray Diffraction (People’s Republic of China, 1997), Vol. 17.

Keywords

X-ray diffraction data of C16H14O4Ru2M (M=Ge,Si)

  • Yu PuLan (a1), Ding Shuang (a1), Qiao YuanYuan (a1), Yao XinKan (a1), Liu Chong (a1) and Lin ShaoFan (a1)...

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