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Powder X-ray diffraction of 5-Chloro-N-(4-nitrophenyl) pentanamide, C11H13ClN2O3

  • Qing Wang (a1), Yan Mei Huang (a1), Qiao Mei Sun (a1), Xiang Ling Ma (a1) and Hui Li (a1)...

Abstract

X-ray powder diffraction data for 5-Chloro-N-(4-nitrophenyl)pentanamide, C11H13ClN2O3, are reported [a = 8.036(4) Å, b = 15.972(5) Å, c = 9.829(5) Å, α = 90°, β = 104.227(2)°, γ = 90°, V = 1222.98 Å3, Z = 4, ρ x = 1.3941 g cm−3 and space group P21/c]. All measured lines were indexed and are consistent with the P21/c space group. No detectable impurities were observed.

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a) Author to whom correspondence should be addressed. Electronic mail: lihuilab@sina.com

References

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Jiang, J. and Ji, Y. (2013). “Alternate synthesis of apixaban (BMS-562247), an inhibitor of blood coagulation factor Xa,” Synth. Commun. 43(1), 7279.
Neumann, M. A. (2003). “X-Cell: a novel indexing algorithm for routine tasks and difficult cases,” J. Appl. Crystallogr. 36, 356365.
Pawley, G. S. (1981). “Unit-cell refinement from powder diffraction scans,” J. Appl. Crystallogr. 14(6), 357361.
Watson, J., Whiteside, G., and Perry, C. (2011). “Apixaban,” Drugs 71, 20792089.

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Supplementary materials

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Table S1

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Powder X-ray diffraction of 5-Chloro-N-(4-nitrophenyl) pentanamide, C11H13ClN2O3

  • Qing Wang (a1), Yan Mei Huang (a1), Qiao Mei Sun (a1), Xiang Ling Ma (a1) and Hui Li (a1)...

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