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Powder X-ray diffraction data for innelite

  • Gunnar Raade (a1) and Hans-Jørgen Berg (a1)

Abstract

X-ray powder data originally published for innelite—Na2Ba3(Ba, K, Mn)(Ca, Na)Ti(TiO2)2[Si2O7]2(SO4)2—were erroneously those of catapleiite. The new data reported here are compared with powder data calculated from the published structure. The cell is triclinic (space group P1, Z=1), a=14.71(1) Å, b=7.115(7) Å, c=5.379(4) Å, α=90.02(7)°, β=94.68(8)°, γ=98.43(9)°, V=555.0(6) Å3, F30=5.2(0.053,109).

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References

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Appleman, D. E., and Evans, Jr., H. T. (1973). “Job 9214: Indexing and least-squares refinement of powder diffraction data,” U.S. Geological Survey, Computer Contribution 20, U.S. National Technical Information Service, Document PB 216 188.
Chernov, A. N., Ilyukhin, V. V., Maksimov, B. A., and Belov, N. V. (1971). “The crystal structure of innelite—Na 2Ba 3(Ba, K, Mn)(Ca, Na)Ti(TiO 2)2[Si 2O 7]2(SO 4)2,”Kristallografiya 16, 87 (English translation inSov. Phys. Crystallogr. 16, 65).
Efimov, A. F., Kravchenko, S. M., and Vlasova, E. V. (1963). “Mineralogy of alkali pegmatites of the Inagli massif,” Trudý IMGRE 16, 141.
Kraus, W., and Nolze, G. (1996). “POWDER CELL—a program for the representation and manipulation of crystal structures and calculation of the resulting X-ray powder patterns,” J. Appl. Crystallogr. 29, 301.
Kravchenko, S. M., Vlasova, E. V., Kazakova, M. E., Ilyukhin, V. V., and Abrashev, K. K. (1961). “Innelite—a new barium silicate,” Dokl. Akad. Nauk SSSR 141, 1198 (English translation in Dokl. Akad. Nauk USSR–Earth Science Section 141, 1297).
Smith, G. S., and Snyder, R. L. (1979). “F N: A criterion for rating powder diffraction patterns and evaluating the reliability of powder-pattern indexing,” J. Appl. Crystallogr. 12, 60.
Strunz, H. (1962). “Isotypie Yoshimurait–Innelit,” N. Jb. Miner. Mh. 260.

Powder X-ray diffraction data for innelite

  • Gunnar Raade (a1) and Hans-Jørgen Berg (a1)

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