Skip to main content Accessibility help
×
Home

JCPDS—International Centre for Diffraction Data round robin study of silver behenate. A possible low-angle X-ray diffraction calibration standard

  • T. N. Blanton (a1), T. C. Huang (a2), H. Toraya (a3), C. R. Hubbard (a4), S. B. Robie (a5), D. Louër (a6), H. E. Göbel (a7), G. Will (a8), R. Gilles (a8) and T. Raftery (a9)...

Abstract

A task group of the JCPDS—International Center for Diffraction Data (ICDD) was established with the charge of investigating the use of silver behenate, CH3(CH2)20COO·Ag, as a possible low-angle calibration standard for powder diffraction applications. Utilizing several data collection and analysis techniques, long-period spacing (d001) values with a range of 58.219–58.480 Å were obtained. Using the same collected data and one data analysis refinement calculation method resulted in dm values with a range of 58.303–58.425 Å. Data collected using a silicon internal standard and the same singular data analysis calculation method provided d001 values with a range of 58.363–58.381 Å.

Copyright

Corresponding author

a) Author to whom correspondence should be addressed: Eastman Kodak Company, Kodak Park B49, Rochester, NY 14652-3712.

References

Hide All
Blanton, T. (1991). “Low-Angle Diffraction Study of Silver Behenate,” presented at the JCPDS-ICDD March Annual Meeting, Concordville, PA, USA.
Dragoo, A. L. (1986). “Standard Reference Materials for X-Ray Diffraction Part I. Overview of Current and Future Standard Reference Materials,” Powder Diffr. 1, 294298.
Huang, T. C., Toraya, H., Blanton, T. N., and Wu, Y. (1993). “X-Ray Powder Diffraction Analysis of Silver Behenate, A Possible Low-Angle Diffraction Standard,” J. Appl. Cryst. 26, 180184.
Hubbard, C. R. (1983). “New Standard Reference Materials for X-Ray Powder Diffraction,” Adv. X-ray Anal. 26, 4551.
International Tables for X-ray Crystallography (1974). (Kynoch Press for the International Union of Crystallography, Birmingham, England) Vol. IV; revised and supplementary tables.
Louër, D. (1991). “Indexing of Powder Diffraction Patterns,” Mat. Sci. Forum 79–82, 1726.
Matthews, F. W., Warren, G. G., and Michell, J. H. (1950). “Derivatives of Fatty Acids: Identification by X-Ray Diffraction Powder Patterns,” Anal. Chem. 22, 514519.
Toraya, H., and Kitamura, M. (1990). “Simultaneous Peak-Shift Correction in the Least-Squares Determination of Unit-Cell Parameters of a Sample with Standard Reference Material,” J. Appl. Cryst. 23, 282285.
Toraya, H. (1993). “The Determination of Unit-Cell Parameters from Bragg Reflection Data Using a Standard Reference Material but without a Calibration Curve,” J. Appl. Cryst. 26, 583590.
Toraya, H. (1994). Private communication.
Wong-Ng, W., and Hubbard, C. R. (1987). “Standard Reference Materials for X-Ray Diffraction Part II. Calibration Using d-Spacing Standards,” Powder Diffr. 2, 242248.

Keywords

JCPDS—International Centre for Diffraction Data round robin study of silver behenate. A possible low-angle X-ray diffraction calibration standard

  • T. N. Blanton (a1), T. C. Huang (a2), H. Toraya (a3), C. R. Hubbard (a4), S. B. Robie (a5), D. Louër (a6), H. E. Göbel (a7), G. Will (a8), R. Gilles (a8) and T. Raftery (a9)...

Metrics

Full text views

Total number of HTML views: 0
Total number of PDF views: 0 *
Loading metrics...

Abstract views

Total abstract views: 0 *
Loading metrics...

* Views captured on Cambridge Core between <date>. This data will be updated every 24 hours.

Usage data cannot currently be displayed