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Xrd and Xtem Investigation of Polycrystalline Silicon Carbide on Polycrystalline Silicon

Published online by Cambridge University Press:  15 February 2011

S. Roy
Affiliation:
Microfabrication Laboratory, Electrical Engineering and Applied Physics, Case Western Reserve University, Cleveland, OH 44106, ro@mems4.cwru.edu
C. A. Zorman
Affiliation:
Microfabrication Laboratory, Electrical Engineering and Applied Physics, Case Western Reserve University, Cleveland, OH 44106, ro@mems4.cwru.edu
C. H. Wu
Affiliation:
Materials Science and Engineering, Case Western Reserve University, Cleveland, OH 44106
A. J. Fleischman
Affiliation:
Microfabrication Laboratory, Electrical Engineering and Applied Physics, Case Western Reserve University, Cleveland, OH 44106, ro@mems4.cwru.edu
M. Mehregany
Affiliation:
Microfabrication Laboratory, Electrical Engineering and Applied Physics, Case Western Reserve University, Cleveland, OH 44106, ro@mems4.cwru.edu
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Abstract

Atmospheric pressure chemical vapor deposition (APCVD) was used to grow silicon carbide (SiC) on as-deposited and annealed polycrystalline silicon (polysilicon) films which were deposited on oxidized Si wafers. X-ray diffraction (XRD) reveals that SiC films grown on asdeposited polysilicon have a (110) orientation. XRD performed on as-deposited polysilicon before and after SiC growth reveals that the orientation of polysilicon changes from (110) to a mixture of (110) and (11) during growth of 2 μm-thick SiC films. Cross-sectional transmission electron microscopy (XTEM) images of the SiC/polysilicon interface show that the SiC appears to be unaffected by the recrystallization of the underlying polysilicon during the SiC growth. XRD from samples of SiC grown on annealed polysilicon show that both films have (110) and (111) orientations. For SiC films grown on annealed polysilicon substrates, XTEM images show that the crystallinity of the annealed polysilicon substrate does not significantly change during SiC growth. Furthermore, an investigation of the SiC/annealed-polysilicon interface using selected area diffraction (SAD) shows that an epitaxial relationship exists between the polysilicon and SiC grains.

Type
Research Article
Copyright
Copyright © Materials Research Society 1997

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