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Transmission Electron Microscopy of Shock-Modified and Annealed Rutile*

  • M. J. Carr (a1), R. A. Graham (a1), B. Morosin (a1) and E. L. Venturini (a1)

Abstract

The annealing behavior of shock modified rutile (TiO2) powder was studied by transmission electron microscopy, x-ray line broadening, and electron spin resonance. Specimens were examined in the as-received and as-shocked conditions, and in shocked and annealed conditions after one hour at 475° or 1000°C. The dislocations generated by the shock treatment were found to persist essentially unaltered through the 475°C anneal. Substantial recovery was observed after the 1000°C anneal.

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This work performed at Sandia National Laboratories supported by the U. S. Department of Energy under Contract No. DE-ACO4-76DP00789.

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1. Batsanov, S. S., Boreskov, G. K., Gridasova, G. V., Keier, N. P., Kefeli, L. M., Kudinov, V. M., Mali, V. G. and Sazonova, I.S., Kinetics and Catalysts 8, 11401146 (1967).
2. Golden, J., Williams, F., Morosin, B., Venturini, E. L. and Graham, R. A. in Shock Waves in Condensed Matter, 1981 (Menlo Park), edited by Nellis, W. J., Seaman, L. and Graham, R. A., American Institute of Physics, New York (1982), pp. 7276.
3. Golden, J., Masters Degree thesis, University of New Mexico, Department of Chemical Engineering (1982).
4. Venturini, E. L., Morosin, B. and Graham, R. A. in Nellis, W. J., et al. eds, loc cit pp. 77–81.
5. Morosin, B. and Graham, R. A. in Proceedings 1983 American Physical Society Topical Conference on Shock Waves in Condensed Matter editors Asay, J. R., Graham, R. A., and Straub, G. K., July 21–23, 1983, Santa Fe, NM (in press).
6. Graham, R. A. and Webb, D. M., in Asay, J. R., et al. , eds., loc cit.

Transmission Electron Microscopy of Shock-Modified and Annealed Rutile*

  • M. J. Carr (a1), R. A. Graham (a1), B. Morosin (a1) and E. L. Venturini (a1)

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