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Production of Nanostructures Under Ultraturbulent Collision Reaction Conditions - Application to Catalysts, Superconductors, CMP Abrasives, Ceramics, and Other Nanoparticles

Published online by Cambridge University Press:  10 February 2011

Irwin J. Gruverman  and
Jeffrey R. Thumm
Irwin J. Gruverman
Affiliation:
Microfluidics Division, MFIC Corporation, 30 Ossipee Road Newton, MA 02464-9101
Jeffrey R. Thumm
Affiliation:
Microfluidics Division, MFIC Corporation, 30 Ossipee Road Newton, MA 02464-9101
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Abstract

The development, operation and applications of a novel continuous chemical reactor system are described. The system, known as a Multiple Stream Mixer/Reactor (or MMR), produces nanoparticles by direct precipitation from two or more reactant solution streams in an extreme energy density, ultraturbulent, collision reaction region. Sensors and a control system are employed to assure constant mixing conditions and desired stoichiometry in the reaction region. The interaction chamber is designed to allow macro-, meso- and micromixing during processing. This allows control of product purity, yield, size, size distribution, and phase purity. Typical nanoparticle diameters in the one to ten nanometer range are often achievable, with tight size distribution. The MMR can be scaled from development quantities to tons/hour for production applications.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 775: Symposium P – Self-Assembled Nanostructured Materials , 2003 , P9.7
Copyright
Copyright © Materials Research Society 2003

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References

1. Kilner, P.H., King, D.L., “Development of Improved Catalysts Using Nanometer-Scale Technology”, Final Report to NIST under ATP Project 94-01-0190, (1998)Google Scholar
2. Ginter, D.M., King, D.L., Kilner, P.H., “Use of a High Intensity Multistream Mixer Reactor for the Precipitation of Catalyst Precursors Having Reduced Crystallite Size and Improved Phase Purity”, Presented at AIChE Symposium on Nano Srtuctured Materials, November, 1998 Google Scholar
3. Ginter, D.M., King, D.L., Kilner, P.H., “Effect of a Novel Multistream Mixer Reactor in Reducing Mass Transfer Limitations in a Model Fast Chemical Reaction”, Presented at AIChE Symposium on Liquid-Liquid and Liquid-Solid Mixing, November, 1998 Google Scholar
4. Gruverman, I. J., Drug Delivery Technology 3, 52 (2003)Google Scholar
5. Bourne, J.R., “Turbulent Mixing and Chemical Reactions” (Wiley, 1999)Google Scholar