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A Preliminary Characterization of the Defect Structure of the Zeta Phase in the Interfacial Region of Fe-Zn Couples

  • Lucille A. Giannuzzi (a1), Paul R. Howell (a1), Howard W. Pickering (a1) and William R. Bitler (a1)

Abstract

A preliminary investigation of the defect structure of the monoclinic zeta phase, within the interfacial region of Fe-Zn couples, has been performed using cross-section transmission electron microscopy (TEM). Twin boundaries and dislocations have been unambiguously identified, however, examples of defects which, as of yet are unknown, are also presented. The monoclinic zeta phase was found to twin by a rotation of 180° about the normal to the (110) plane.

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[1] Giannuzzi, L. A., Howell, P. R., Pickering, H. W., and Bider, W. R., to be published, Proceedings of the American Electroplaters and Surface Finishers Society, SUR/FIN ‘91, Toronto, June 1991.
[2] Giannuzzi, L. A., Howell, P. R., Pickering, H. W., and Bider, W. R., to be published, Proceedings of the ASTM STP Symposium on Metallography: 75 Years Later, Atlantic City, May 1991.
[3] Goodhew, P.J., “Thin Foil Preparation for Electron Microscopy”, in Practical Methods in Electron Microscopy, vol.11, ed. Glauert, A.M., Elsevier, Amsterdam, (1985), 110.
[4] Gellings, P. J., Bree, E. W. d., Gierman, G., Z. Metallkd., 70, (1979), 315.
[5] Hirsch, P., Howie, A., Nicholson, R. B., Pashley, D. W., and Whelan, M. J., Electron Microscopy of Thin Crystals, 2nd ed., Krieger, R. E. Publishing Co., Florida, (1977), 271272.
[6] Hirsch, P., Howie, A., Nicholson, R. B., Pashley, D. W., and Whelan, M. J., Electron Microscopy of Thin Crystals, 2nd ed., Krieger, R. E. Publishing Co., Florida, (1977) 185188.

A Preliminary Characterization of the Defect Structure of the Zeta Phase in the Interfacial Region of Fe-Zn Couples

  • Lucille A. Giannuzzi (a1), Paul R. Howell (a1), Howard W. Pickering (a1) and William R. Bitler (a1)

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