Hostname: page-component-77c89778f8-gq7q9 Total loading time: 0 Render date: 2024-07-20T18:04:18.376Z Has data issue: false hasContentIssue false

Poly(Vinyl Butyral) Pyrolysis: Interactions with Plasticizer and Ain Ceramic Powder

Published online by Cambridge University Press:  25 February 2011

H. Yan
Affiliation:
Rutgers University, New Brunswick, NJ 08855-0909
W. R. Cannon
Affiliation:
Rutgers University, New Brunswick, NJ 08855-0909
D. J. Shanefield
Affiliation:
Rutgers University, New Brunswick, NJ 08855-0909
Get access

Abstract

TGA and FTIR were employed to investigate the effects of dibutyl phthalate and butyl benzyl phthalate on the thermal degradation behavior of PVB, a binder used commonly for tape casting. Butyl benzyl phthalate was found to enhance the crosslinking of the PVB binder when heated in a nitrogen atmosphere during binder pyrolysis, which retarded its thermal degradation.

The interaction between AIN powder and PVB binder was also studied by using TGA, XPS and a special furnace for collecting residual carbon. Intrinsic char and gas phase mediated char were studied separately.

Type
Research Article
Copyright
Copyright © Materials Research Society 1992

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

[1] Mistler, R. E., Shanefield, D. J. and Runk, R. B., in Ceramic Processing before Firing, edited by Onoda, G. Y. and Hench, L. L., (John Wiley, New York, 1978), pp. 411448.Google Scholar
[2] Shih, W. K., Sacks, M. D. etc., Ceram Trans, I ( Ceramic Powder Sci. 2, Pt. A), 549558 (1988).Google Scholar
[3] Whitman, D., in ISHM'88 proceedings, (1988), pp. 421425.Google Scholar