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Multilayer Precursor Synthesis of New Copper-Tungsten Selenides

  • Loreli Fister (a1), Marc D. Hornbostel (a1) and David C. Johnson (a1)

Abstract

We have made new ternary compounds in the copper tungsten selenium system using multilayer thin films as reactants. The compounds appear to be unstable above temperatures near 1000ºC with respect to binary compounds, which helps to explain the difficulty in making these compounds by conventional methods.

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[2] Warren, John L. and Geballe, Theodore H.. Research opportunities in new energy-related materials. Materials Science and Engineering, 50:149198, 1981.
[3] Fukuto, Masafumi, Hornbostel, Marc D., and Johnson, David C.. The use of superlattice structure to control reaction mechanism: The kinetics and energetics of Nb5Se4formation. Journal of the American Chemical Society, 116:91369140, 1994.
[4] Fister, Loreli, Johnson, David C., and Brown, Robert. Synthesis of CuxMo6Se8 without binary compounds as intermediates: A study using superlattices to kinetically control a solid-state reaction. Journal of the American Chemical Society, 116:629633, 1994.
[5] Fister, Loreli and Johnson, David C.. Controlling solid-state reaction mechanisms using diffusion length in ultrathin-film superlattice composites. Journal of the American Chemical Society, 114:46394644, 1992.
[6] Fister, Loreli, Li, Xiao-Mei, McConnell, John, Novet, Thomas, and Johnson, David C.. Deposition system for the synthesis of modulated, ultrathin-film composites. Journal of Vacuum Science and Technology A, 11(6):30143019, 1993.
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[9] Bird, D. M. and Saunders, M.. Inversion of convergent-beam electron diffraction patterns. Acta Crystallographica, A48:555562, 1992.

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Multilayer Precursor Synthesis of New Copper-Tungsten Selenides

  • Loreli Fister (a1), Marc D. Hornbostel (a1) and David C. Johnson (a1)

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