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Microstrucrure and Properties of In-Situ R. F. Sputtered YBa2Cu3O7−x Thin Films for Microwave Applications

Published online by Cambridge University Press:  26 February 2011

David W. Reagor
Affiliation:
Los Alamos National Laboratory, Los Alamos, NM 87545.
Margarita E. Piza
Affiliation:
Dept. Materials Science, Massachussetts Institute of Technology
Robert J. Houlton
Affiliation:
Los Alamos National Laboratory, Los Alamos, NM 87545.
Fernando H. Garzon
Affiliation:
Los Alamos National Laboratory, Los Alamos, NM 87545.
Marilyn Hawley
Affiliation:
Los Alamos National Laboratory, Los Alamos, NM 87545.
Ian D. Raistrick
Affiliation:
Los Alamos National Laboratory, Los Alamos, NM 87545.
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Abstract

The residual surface resistance of a number of films of YBa2Cu3O7−x, prepared by off-axis sputtering onto MgO substrates, has been measured using a parallel-plate resonator technique. Deposition conditions were kept constant, apart from the substrate temperature. There is no correlation between surface resistance and other important microscopic parameters, such as Tc and c-axis lattice parameter. There is, however, a trend to higher Rs with increasing volume fraction of in-plane misoriented material, although the correlation is not perfect. Furthermore, we have found that most of the misoriented material is localized at the film substrate interface and, therefore, is probably not responsible for most of the RF losses. The data suggest that at higher deposition temperatures, there is an increasing tendency for 45° misoriented material to appear in the films, and a significant fraction of this material may be present closer to the free film surface. Scanning Tunneling Microscopy (STM) qualitatively supports this conclusion.

Type
Research Article
Copyright
Copyright © Materials Research Society 1992

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References

REFERENCES

1. Laderman, S. S., Taber, R. C., Jacowitz, R. D., Moll, J. L., Eom, C. B., Hylton, T. L., Marshall, A. F., Geballe, T. H., and Beasley, M. R., “Resistive loss at 10 GHz in c-axis-aligned in-situ-grovm YBa2Cu3O7−x, films,” Rev. 43, 2922 (1991).Google Scholar
2. Eom, E. B., Sun, J. Z., Lairson, B. M., Streiffer, S. K., Marshall, A. F., Yamamoto, K., “Synthesis and properties of YBa2Cu3O7 thin films grown in situ by 90° off-axis single magnetron sputtering,” Physica C 171, 354 (1990).Google Scholar
3. Enprotech Corp., 1 Station Square, Suite 620, Pittsburgh, P. A. 15219.Google Scholar
4. Tabor, R. C., “A parallel plate resonator technique for microwave loss measurements on superconductors,” Rev. Sci. Instr., 61, 2200 (1990).Google Scholar
5. Halbritter, J.RF residual losses, surface impedance, and granularity in superconducting cuprates,” J. Appl. Phys, 68, 6315 (1990).Google Scholar
6. Raistrick, Ian. D., Hawley, Marilyn, Beery, Jerome, Garzon, Fernando and Houlton, Robert J.Microstructure and growth mechanism of thin sputtered films of YBa2Cu3O7 on MgO substrates,” Appl. Phys. Lett, 59, 3177 (1991).Google Scholar