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Measurement of Crystal Lattice Rotations under Nanoindents in Copper

Published online by Cambridge University Press:  01 February 2011

Kirsten K. McLaughlin ,
Nadia A. Stelmashenko ,
Stephen J. Lloyd ,
Luc J. Vandeperre  and
William J. Clegg
Kirsten K. McLaughlin
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Pembroke Street, Cambridge, CB2 3QZ, UK.
Nadia A. Stelmashenko
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Pembroke Street, Cambridge, CB2 3QZ, UK.
Stephen J. Lloyd
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Pembroke Street, Cambridge, CB2 3QZ, UK.
Luc J. Vandeperre
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Pembroke Street, Cambridge, CB2 3QZ, UK.
William J. Clegg
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Pembroke Street, Cambridge, CB2 3QZ, UK.
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Abstract

A technique is described to measure the rotations of the crystal lattice in the deformed region around a nanoindent from volumes smaller than 3 × 10−5 μm3. To demonstrate this method, a copper crystal has been indented on its (001) face to depths of 500 and 1300 nm. Cross-sections of nanoindents were prepared for transmission electron microscopy by focused ion beam milling, and rotations were measured about the [001], [010] and [100] axes using convergent beam electron diffraction.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 841: Symposium R – Fundamentals of Nanoindentation and Nanotribology III , 2004 , R1.3
Copyright
Copyright © Materials Research Society 2005

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References

REFERENCES

1. Johnson, K.L., Contact Mechanics. (Cambridge University Press, Cambridge, 1985) p. 174.Google Scholar
2. Wang, Y., Raabe, D., Klüber, C. and Roters, F.. Acta mater. 52, 2229 (2004).Google Scholar
3. Fleck, N.A., Muller, G.M., Ashby, M.F. and Hutchinson, J.W.. Acta metall. mater. 42, 475 (1994).Google Scholar
4. Gao, H., Huang, Y. and Nix, W.D.. Naturwissenchaften. 86, 507 (1999).Google Scholar
5. Jayaweera, N.B., Downes, J.R., Frogley, M.D., Hopkinson, M., Bushby, A.J., Kidd, P., Kelly, A. and Dunstan, D.J.. Proc. Roy. Soc. Lond. A. 459 (2036), 2049 (2003).Google Scholar
6. Read, D., Geiss, R., Ramsey, J., Scherban, T., Xu, G., Blane, J., Miner, B. and Emery, R. D. in Mechanical Properties Derived from Nanostructuring Materials, edited by Bahr, D.F., Kung, H., Moody, N.R. and Wahl, K.J., (Mater. Res. Soc. Symp. Proc. 778, San Francisco CA, 2003) pp. 93–98.Google Scholar
7. Stelmashenko, N.A., Walls, M.G., Brown, L.M. and Milman, Yu. V.. Acta metall. mater. 41 (10), 2855 (1993).Google Scholar
8. Harvey, S., Huang, H., Venkataraman, S. and Gerberich, W.W.. J. Mater. Res. 8 (6), 1291 (1993).Google Scholar
9. Zielinski, W., Huang, H. and Gerberich, W.W.. J. Mater. Res. 8 (6), 1300 (1993).Google Scholar
10. Stelmashenko, N.A. and Brown, L.M.. Phil. Mag. 74 (5), 1195 (1996).Google Scholar
11. Nye, J.F.. Acta metall. 1, 153 (1953).Google Scholar
12. Yang, W., Larson, B.C., Pharr, G.M., Ice, G.E., Budai, J.D., Tischler, J.Z. and Liu, W.. J. Mater. Res. 19 (1), 66 (2004).Google Scholar
13. Yang, W., Larson, B.C., Tischler, J.Z., Ice, G.E., Budai, J.D. and Liu, W.. Micron. 35, 431 (2004).Google Scholar
14. Lloyd, S. J., Molina-Aldareguia, J. M. and Clegg, W. J.. Philos. Mag. A. 82 (10), 1963 (2002).Google Scholar
15. Wang, S.C. and Starink, M.J.. J. Microsc. 211 (2), 130 (2003).Google Scholar