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Investigations of Microstructural Changes in Nickel Thin Films on Ionimplanted Silicon by Cross-Sectional Transmission Electron Microscopy with Intermittent Annealings in N2 Ambient

Published online by Cambridge University Press:  25 February 2011

S. W. Lu
Affiliation:
Department of Materials Science and Engineering, National Tsing Hua University, Hsinchu, Taiwan, Republic of China
C. W. Nieh
Affiliation:
Department of Materials Science and Engineering, National Tsing Hua University, Hsinchu, Taiwan, Republic of China
C. S. Chang
Affiliation:
Department of Materials Science and Engineering, National Tsing Hua University, Hsinchu, Taiwan, Republic of China
L. J. Chen
Affiliation:
Department of Materials Science and Engineering, National Tsing Hua University, Hsinchu, Taiwan, Republic of China
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Abstract

The feasibility of studying dynamical changes in nickel thin films on ion-implanted silicon thin films by cross-sectional transmission electron microscopy (XTEM) with intermittent annealings in N2 ambient up to 850 °C is demonstrated. Interactions of nickel thin films with oxidation induced stacking faults, fluorine bubbles and process-induced defects in ion implanted silicon are provided as examples. The technique may be applied to clarify a number of important issues encountered in the study of the reactions and diffusion of thin films and obtain informations otherwise unattainable.

Type
Research Article
Copyright
Copyright © Materials Research Society 1987

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References

REFERENCES

1. Tu, K.N. and Mayer, J.W., in Thin Films — Interdiffusion and Reactions, edited by Poate, J.M., Tu, K.N., and Mayer, J.W. (Wiley, New York, 1978), p. 359.Google Scholar
2. Thomas, G. and Goringe, M.J., Transmission Electron Microscopy of Materials (Wiley-Interscience, New York, 1979).Google Scholar
3. Marcus, R.B. and Sheng, T.T., Transmission Electron Microscopy of Silicon VLSI Circuits and Structures (Wiley-Interscience, New York, 1983).Google Scholar
4. Bulter, E.P. and Hale, K.F., Dynamical Experiments in the Electron Microscope (North-Holland, Amsterdam, 1981).Google Scholar
5. Smith, D.A., Psaras, F.A., Fisher, I.J., and Tu, K.N., Mater. Res. Soc. Symp. Proc. 37, 407 (1985).Google Scholar
6. Ohdomari, I., Konuma, K., Takano, M., Chikyow, T., Kawarada, H., Nakanishi, J., and Ueno, T., Mater. Res. Soc. Symp. Proc. 54, 63 (1986).Google Scholar
7. Chen, L.J., Wu, Y.J., and Wu, I.W., J. Appl. Phys. 52, 3520 (1981).Google Scholar
8. Nieh, C.W. and Chen, L.J., Appl. Phys. Lett. 48, 1528 (1986).Google Scholar
9. Sheng, T.T. and Chang, C.C., IEEE Trans. Electron Devices ED–23, 531 (1976).Google Scholar
10. Tu, K.N., Alessandrini, E.I., Chu, W.K., Krautle, H., and Mayer, J.W., Jpn. J. Appl. Phys. 2, Supple. 2–1, 669 (1974).Google Scholar
11. Lu, S.W., Nieh, C.W., and Chen, L.J., J. Appl. Phys. (In Press, 1987).Google Scholar
12. Nieh, C.W. and Chen, L.J., J. Appl. Phys. 60, 3114 (1986).Google Scholar
13. Nieh, C.W. and Chen, L.J., J. Appl. Phys. 60, 3546 (1986).Google Scholar
14. Chen, L.J. and Hou, C.Y., Chinese J. Mater. Sci. 15–1, 1 (1983).Google Scholar