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Investigation of Interfaces in Ceramics by Electron Spectroscopic Imaging

  • J. Mayer (a1), J. Plitzko (a1), F. Steinbach (a1) and H. Kohl (a2)

Abstract

Electron Spectroscopic Imaging (ESI) in an energy filtering TEM is a new analytical technique which allows one to obtain two-dimensional elemental distribution images. In the present paper the detection limits of the new technique will be discussed. Si3N4 ceramics with different thicknesses of the amorphous oxide grain boundary layers have been chosen as a model system. Quantitative results have been obtained on three different energy filtering instruments and will be compared with the results of theoretical calculations. The application of ESI for the mapping of near edge fine structure will be discussed.

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1. Lanio, S., Rose, H., and Krahl, D., Optik 73, 56 (1986).
2. Krivanek, O.L., Gubbens, A.J., Dellby, N., and Meyer, C.E., MMM 3, 187 (1992).
3. Strecker, A., Salzberger, U., and Mayer, J., Pract. Metallography 30, 482 (1993).
4. Jeanguillaume, C., Trebbia, P., and Colliex, C., Ultramicroscopy 3, 237 (1978).
5. Egerton, R.F., Electron Energy Loss Spectroscopy in the Electron Microscope, Plenum Press, New York (1986).
6. Weickenmeier, A., Nüchter, W., and Mayer, J., Optik, to be published.
7. Berger, A., and Kohl, H., Optik 92, 175 (1993).
8. Clarke, D.R., J. Am. Cer. Soc. 70, 15 (1987).
9. Kleebe, H.J., Cinibulk, M.K., Cannon, R.M., and Rühle, M., J. Am. Cer. Soc. 76, 1969 (1993).
10. Cinibulk, M.K., Kleebe, H.J., and Rühle, M., J. Am. Cer. Soc. 76, 426 (1993).
11. Tanaka, I., Kleebe, H.J., Cinibulk, M.K., Bruley, J., Clarke, D.R., and Rühle, M., J. Am. Cer. Soc., in press (1994).
12. Berger, A., Mayer, J., and Kohl, H., Ultramicroscopy 55, 101 (1994).
13. Rösler, M., Zachai, R., Füβer, H.-J., Jiang, X., Klages, C.-P., Proc. 2nd Int. Conf. Applications Diamond Films and Related Mat., Yoshikawa, M., Murakawa, M., Eds., Tokyo, (1993).

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