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High Temperature X-Ray Diffraction in Transmission Under Controlled Environment

Published online by Cambridge University Press:  10 February 2011

L. Margulies ,
M. J. Kramer ,
J. J. Williams ,
E. M. Deters ,
R. W. McCallum ,
D. R. Haeffner ,
J. C. Lang ,
S. Kycia  and
A. I. Goldman
L. Margulies
Affiliation:
Ames Laboratory, Iowa State University, Ames, IA 50011, hanuman@iastate.edu
M. J. Kramer
Affiliation:
Ames Laboratory, Iowa State University, Ames, IA 50011
J. J. Williams
Affiliation:
Ames Laboratory, Iowa State University, Ames, IA 50011
E. M. Deters
Affiliation:
Ames Laboratory, Iowa State University, Ames, IA 50011
R. W. McCallum
Affiliation:
Ames Laboratory, Iowa State University, Ames, IA 50011
D. R. Haeffner
Affiliation:
APS, Argonne National Laboratory, Argonne, II 60439
J. C. Lang
Affiliation:
APS, Argonne National Laboratory, Argonne, II 60439
S. Kycia
Affiliation:
CHESS, Cornell University, Ithaca, NY 14853
A. I. Goldman
Affiliation:
Ames Laboratory, Iowa State University, Ames, IA 50011
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Abstract

A compact tube furnace has been developed for high temperature X-ray diffraction studies using high energy synchrotron radiation. The furnace design has a low absorption path in transmission yet allows for a high degree of control of the sample atmosphere and a minimal temperature gradient across the sample. The design allows for a maximum temperature of 1500°C with a variety of atmospheres including inert, reducing, and oxidizing. Preliminary results obtained at the SRI-CAT I-ID undulator line (60keV) at the APS facility and the A2 24 pole wiggler line (45keV) at CHESS on the Ti5Si3Z5 (Z = C, N, O) system will be presented to demonstrate the feasibility of this approach.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 524: Symposium V – Application of Synchrotron Radiation Techniques…IV , 1998 , 139
Copyright
Copyright © Materials Research Society 1998

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References

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