Hostname: page-component-8448b6f56d-t5pn6 Total loading time: 0 Render date: 2024-04-18T10:20:29.662Z Has data issue: false hasContentIssue false

Atomic Resolution Imaging of Surfaces By Electron Microscopy

Published online by Cambridge University Press:  26 February 2011

David J. Smith*
Affiliation:
Center for Solid State Science and Department of Physics Arizona State University, Tempe, Arizona B5287.
Get access

Abstract

The electron microscope can be operated in several different modes to provide atomic-level detail about surfaces. The REM technique with glancing-angle incidence permits the topography of bulk surfaces to be characterized with a resolution of better than 10A, and atomic-step-height features are visible. The standard TEM bright- and dark-field modes can also be used with appropriate samples to provide monolayer sensitivity. The profile imaging technique is ideal for following real-time dynamic processes. Typical vacuum levels ( ∼10−7 torr), and the lack of facilities for surface cleaning, currently impose a restriction on the materials which can be usefully studied in most available microscopes. Clean and well-defined environments for the sample, without any compromise of the microscope performance, will become increasingly common in the near future.

Type
Research Article
Copyright
Copyright © Materials Research Society 1987

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Golovchenko, J.A., these proceedings.Google Scholar
2. Cowley, J.M., Progress Surf. Sci. 21, 209 (1986).CrossRefGoogle Scholar
3. Tanishiro, Y., Takayanagi, K. & Yacri, K.,J. Micros. 142,211(1986).CrossRefGoogle Scholar
4. Uchida, Y., Lemphfuhl, G. and Jager, J., Ultramicroscopy 15, 119 (1984).CrossRefGoogle Scholar
5. Hsu, Tung, Ultramicroscopy 11, 167 (1983).CrossRefGoogle Scholar
6. Lemphfuhl, G. and Uchida, Y., Ultramicroscopy 4, 275 (1979).CrossRefGoogle Scholar
7. Klaua, M. and Bethge, H., Ultramicroscopy 11, 125 (1983).CrossRefGoogle Scholar
8. Takayanagi, K., Kobayashi, K., Kodoira, Y., Yokoyama, Y. and Yagi, K., Proc. 7th Int. Conf. HVEM (Berkeley, 1983) pp. 4752.Google Scholar
9. Cherns, D., Phil. Mag., 30, 549 (1974).CrossRefGoogle Scholar
10. Marks, L.D. and Smith, D.J.. Nature 303, 316 (1983).CrossRefGoogle Scholar
11. Smith, D.J., J. Vac. Sci. Tech. B3, 1563 (1985).CrossRefGoogle Scholar
12. Smith, D.J., in Chemistry and Physics of Solid Surfaces VI (Springer, Heidelberg, 1986) Chapter 15.Google Scholar
13. Smith, D.J., Bursill, L.A. and Jefferson, D.A., Surf. Sci. 175, 673 (1986).CrossRefGoogle Scholar
14. Marks, L.D., Surf. Sci., 139, 281 (1984).CrossRefGoogle Scholar
15. Sinclair, R., Yamashita, T. and Ponce, F.A.,Nature 290,386(1981).CrossRefGoogle Scholar
16. Gibson, J.M., McDonald, M.L. and Untewald, F.C, Phys. Rev. Letts. 55, 1765 (1985).CrossRefGoogle Scholar
17. Yamamoto, N. and Spence, J.C.H., Thin Solid Films 104,43(1983).CrossRefGoogle Scholar
18. Osakabe, N., Tanishiro, Y., Yagi, K. and Honjo, G., Surf. Sci. 97, 393 (1980); Surf. Sci. 102, 424 (1984).CrossRefGoogle Scholar
19. Osakabe, N., Tanishiro, Y., Yaci, K. and Honjo, G., Surf. Sci. 109, 353 (1981).CrossRefGoogle Scholar
20. Shimizu, N., Tanishiro, Y., Kobayashi, K., Takayanagi, K. and Yagi, K., Ultramicroscopy 18, 453 (1985).CrossRefGoogle Scholar
21. Lodge, E.A. and Cowley, J.M., Ultramicroscopy, 13, 213 (1984).CrossRefGoogle Scholar
22. Ye, H.Q. and Smith, D.J., Electron Microscopy 1986, Vol. 2,Google Scholar
23. Hsu, Tung, Ultramicroscopy 11, 167 (1983).CrossRefGoogle Scholar
24. Smith, D.J. and Marks, L.D., Ultramicroscopy 16, 101 (1985).CrossRefGoogle Scholar
25. Hasegawa, T., Kobayashi, K., Ikarashi, N., Takayanagi, K. and Yacri, K., Japan. J. Appl. Phys. 25, L366 (1986).CrossRefGoogle Scholar
26. Petford-Long, A.K. and Smith, D.J., Phil. Mag. A54, 857(1986).Google Scholar
27. Ehrlich, D.J. and Smith, D.J., Appl. Phys. Letts., 48,1751(1986).CrossRefGoogle Scholar
28. Smith, D.J. and Bursill, L.A., Ultramicroscopy 17, 285 (1985).CrossRefGoogle Scholar
29. Petford, A.K., Marks, L.D. and O'Keeffe, M., Surf. Sci. 172, 496 (1986).CrossRefGoogle Scholar
30. Smith, D.J., McCartney, M.R. and Bursill, L.A., Ultramicroscopy, in press.Google Scholar
31. Lin, T.T. and Lichtman, D., J. Mats. Sci. 14, 455 (1979).CrossRefGoogle Scholar
32. lijima, S. and Ichihashi, T., Phys. Rev. Lett., 56, 616 (1986).Google Scholar
33. Smith, D.J., Petford-Long, A.K., Wallenberg, L.R. and Bovin, J.-O., Science 233, 872 (1986).CrossRefGoogle ScholarPubMed
34. Bovin, J.-O., Wallenberg, L.R. & Smith, D.J.,Nature 317,47(1985).CrossRefGoogle Scholar
35. Takayanagi, K., J. Microscopy 136, 287 (1985).CrossRefGoogle Scholar