Hostname: page-component-848d4c4894-tn8tq Total loading time: 0 Render date: 2024-06-23T18:22:18.009Z Has data issue: false hasContentIssue false

An in Situ High Voltage Electron Microscopy Technique for the Study of Deformation and Fracture: in Multilayered Materials

Published online by Cambridge University Press:  15 February 2011

M.A. Wall
Affiliation:
Chemistry and Materials Science Department, L-350, Lawrence Livermore National Laboratory Livermore, CA. 94550.
T.W. Barbee Jr.
Affiliation:
Chemistry and Materials Science Department, L-350, Lawrence Livermore National Laboratory Livermore, CA. 94550.
T.P. Weihs
Affiliation:
Chemistry and Materials Science Department, L-350, Lawrence Livermore National Laboratory Livermore, CA. 94550.
Get access

Abstract

A novel, in situ, high voltage electron microcopy technique for the direct observation of the micromechanisms of tensile deformation and fracture in nanostructured materials is detailed. This technique is particularly well suited for the dynamic observations of deformation and fracture in multilayered materials. The success of this type of in situ technique is highly dependent upon unique specimen preparation procedures and sample design, the importance thereof will be discussed. The initial observations discussed here are expected to aid in our understanding of the mechanical behavior of this new class of atomically engineered materials.

Type
Research Article
Copyright
Copyright © Materials Research Society 1995

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1) Butler, E. P., in Proceedings of the 38th Electron Microscopy Society of America, (Claton Publishing Div., Baton Rouge, Louisiana, 1980), p. 1215.Google Scholar
2) Suryananayana, C. and Froes, F.H., Metallurgical Transactions A, 23A: 10711081, (1992).Google Scholar
3) Grilhe, J., in Mechanical properties and deformatiom behavior of materials having ultra-fine microstructures, (Kluwer Academic Publishers, Boston, Ma, 1993), p. 255286.Google Scholar
4) Messerschmidt, U., (1989) Electron microscopy in plasticity and fracture research of materials, (Akademie-Verlag Publishers, Berlin).Google Scholar
5) Weihs, T.P., Wall, M.A. and Barbee, T.W. Jr., in Proceedings of the Materials Research Society Symposium, (Mater. Res. Soc. Proc. 308, Vol. 308, 1994), p. 753758.Google Scholar
6) Wall, M.A., Microscopy Research and Technique, 27:262267, (1994).Google Scholar
7) Butler, E. P., in Proceedings of the 47th annual meeting of the electron microscopy society for america, (San Francisco Press publishers, San Francisco Ca, 1989). p. 610611.Google Scholar