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UHV Microscopy of the Reconstructed Au (001) Surface

Published online by Cambridge University Press:  22 February 2011

D. N. Dunn
Affiliation:
Department of Materials Science And Engineering, Northwestern University, 2145 Sheridan Road Evanston, III. 60208
L. D. Marks
Affiliation:
Department of Materials Science And Engineering, Northwestern University, 2145 Sheridan Road Evanston, III. 60208
J. P. Zhang
Affiliation:
Department of Materials Science And Engineering, Northwestern University, 2145 Sheridan Road Evanston, III. 60208
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Abstract

We investigate the evolution of the microstructure of a reconstructed Au (001) single crystal surface using ultra high vacuum transmission electron microscopy (UHV-TEM). Bulk single crystal Au (001) surfaces were prepared via standard metallographic techniques and sputter anneal cycles. After a clean surface was obtained, the (001) surface was found to reconstruct into two nearly orthogonal domains of dimensions (5 × ∼ 20 ) along the <110> directions of the unreconstructed F.C.C. (001) surface. Transmission electron diffraction patterns (TED) and dark field microscopy are the two primary techniques used to determine the symmetry and dimensions of the reconstructed surface.

Type
Research Article
Copyright
Copyright © Materials Research Society 1991

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References

[1] Fedak, D.G. and Gjostein, N.A., Acta Metallurgica 15, 827 (1967).CrossRefGoogle Scholar
[2] Fedak, D.G. and Gjostein, N.A., Surface Science 8, 77 (1967).CrossRefGoogle Scholar
[3] Van Hove, M.A., Koestner, R.J., et. al., Surface Science 103, 189 (1981).CrossRefGoogle Scholar
[4] Rieder, K.H., Engel, T., Swendsen, R.H., Surface Science. 127, 223 (1983).CrossRefGoogle Scholar
[5] Yamazaki, K., Takayanagi, K., et. al., Surface Science 199, 595 (1988).CrossRefGoogle Scholar

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