Skip to main content Accessibility help
×
Home
Hostname: page-component-684bc48f8b-zqvvz Total loading time: 0.3 Render date: 2021-04-12T16:53:04.453Z Has data issue: true Feature Flags: { "shouldUseShareProductTool": true, "shouldUseHypothesis": true, "isUnsiloEnabled": true, "metricsAbstractViews": false, "figures": false, "newCiteModal": false, "newCitedByModal": true }

Transmission Electron Microscopy and Electron Holography of Nanophase TiO2 Generated in a Flame Burner System

Published online by Cambridge University Press:  10 February 2011

S. Turner
Affiliation:
Chemical Science and Technology Laboratory;, National Institute of Standards and Technology, Gaithersburg, MD 20899
J. E. Bonevich
Affiliation:
Materials Science and Engineering Laboratory; National Institute of Standards and Technology, Gaithersburg, MD 20899
J. E. Maslar
Affiliation:
Chemical Science and Technology Laboratory;, National Institute of Standards and Technology, Gaithersburg, MD 20899
M. I. Aquino
Affiliation:
Chemical Science and Technology Laboratory;, National Institute of Standards and Technology, Gaithersburg, MD 20899
M. R. Zachariah
Affiliation:
Chemical Science and Technology Laboratory;, National Institute of Standards and Technology, Gaithersburg, MD 20899
Get access

Abstract

Nanophase TiO2 (n-TiO2) particles were generated in a flame burner system under three experimental conditions. Selected individual nanoparticles were identified and characterized using selected area electron diffraction, bright-field and, in some cases, dark-field imaging to determine morphology and microstructural features. Previously unknown TiO2 particles with unusual central features were identified as rutile. Electron holography was used to characterize the central features which were found to be consistent with voids. More extensive characterization of individual particles may lead to improved understanding of n-TiO2 nucleation and growth.

Type
Research Article
Copyright
Copyright © Materials Research Society 1997

Access options

Get access to the full version of this content by using one of the access options below.

References

1. Beck, D.D. and Siegel, R.W., J. Mater. Res. 7, p. 2840 (1992).CrossRefGoogle Scholar
2. Siegel, R.W., Ramasamy, S., Hahn, H., Zongquan, L., Ting, L. and Gronsky, R., J. Mater. Res. 3, p. 1367 (1988).CrossRefGoogle Scholar
3. Hahn, H. and Averback, R.S., J. Am. Chem. Soc. 74, p. 2918 (1991).Google Scholar
4. Shirkhanzadeh, M., Nanostructured Mater. 5, p. 33 (1995).CrossRefGoogle Scholar
5. Akhtar, M.K. and Pratsinis, S.E., J. Am. Ceram. Soc. 75, p. 3408 (1992).CrossRefGoogle Scholar
6. Terwilliger, C.D. and Chiang, Y.M., Nanostructur. Mater. 1, p. 419 (1992).Google Scholar
7. Yang, G., Zhuang, H. and Biswas, P., Nanostructur. Mater. 7, p. 675 (1996).CrossRefGoogle Scholar
8. Formenti, M., Juillet, F., Meriaudeau, P., Teichner, S.J. and Vergnon, P. in Aerosols and Atmospheric Chemistry, edited by Hidy, G.M. (Academic Press, NY, NY, 1972) pp. 4555.CrossRefGoogle Scholar
9. Juillet, F., Lecomte, F., Mozzanega, H., Teichner, S.J., Thevenet, A. and Vergnon, P., Farad. Symp. Chem. Soc. 7, p. 57 (1973).CrossRefGoogle Scholar
10. George, A.P., Murley, R.D. and Place, E.R., Farad. Symp. Chem. Soc. 7, p. 63 (1973).CrossRefGoogle Scholar
11. Bonevich, J.E., Pozzi, G. and Tonomura, A. in Introduction to Electron Holography, edited by Allard, L. et al. (Elsevier Press, Amsterdam, 1996) in press.Google Scholar
12. Deer, W.A., Howie, R.A., and Zussman, J., Rock-Forming Minerals Vol. 5 Non-Silicates, Longman Group LTD, London, 1962, pp. 3443.Google Scholar
13. Allard, L.F., Volkl, E., Kalakkad, D. and Datye, A.K., J. Mater. Sci. 29, p. 5612 (1994).CrossRefGoogle Scholar

Full text views

Full text views reflects PDF downloads, PDFs sent to Google Drive, Dropbox and Kindle and HTML full text views.

Total number of HTML views: 0
Total number of PDF views: 2 *
View data table for this chart

* Views captured on Cambridge Core between September 2016 - 12th April 2021. This data will be updated every 24 hours.

Send article to Kindle

To send this article to your Kindle, first ensure no-reply@cambridge.org is added to your Approved Personal Document E-mail List under your Personal Document Settings on the Manage Your Content and Devices page of your Amazon account. Then enter the ‘name’ part of your Kindle email address below. Find out more about sending to your Kindle. Find out more about sending to your Kindle.

Note you can select to send to either the @free.kindle.com or @kindle.com variations. ‘@free.kindle.com’ emails are free but can only be sent to your device when it is connected to wi-fi. ‘@kindle.com’ emails can be delivered even when you are not connected to wi-fi, but note that service fees apply.

Find out more about the Kindle Personal Document Service.

Transmission Electron Microscopy and Electron Holography of Nanophase TiO2 Generated in a Flame Burner System
Available formats
×

Send article to Dropbox

To send this article to your Dropbox account, please select one or more formats and confirm that you agree to abide by our usage policies. If this is the first time you use this feature, you will be asked to authorise Cambridge Core to connect with your <service> account. Find out more about sending content to Dropbox.

Transmission Electron Microscopy and Electron Holography of Nanophase TiO2 Generated in a Flame Burner System
Available formats
×

Send article to Google Drive

To send this article to your Google Drive account, please select one or more formats and confirm that you agree to abide by our usage policies. If this is the first time you use this feature, you will be asked to authorise Cambridge Core to connect with your <service> account. Find out more about sending content to Google Drive.

Transmission Electron Microscopy and Electron Holography of Nanophase TiO2 Generated in a Flame Burner System
Available formats
×
×

Reply to: Submit a response


Your details


Conflicting interests

Do you have any conflicting interests? *