Published online by Cambridge University Press: 21 February 2011
In attempt to ultimately control the characteristics of the PZT films, we have decided to investigate some of the basic chemistry associated with these solutions. Frequently, these solutions have been generated from Group IV metal alkoxides in acetic acid (HOAc). Therefore, studies of the simple reactivity between M(OCHMe2)4 (M = Ti, Zr) and HOAc have been undertaken. These reactions were monitored by 1H, 13C, 17O NMR, FT-IR, TGA/DTA, and single crystal X‐ray studies. Films were produced from spin‐coat deposition of crystalline material (from the titanium reaction) in toluene and aged solutions as well.
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