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Flux-Assisted Preparation of Powdered Bismuth Superconductors

Published online by Cambridge University Press:  28 February 2011

R. H. Arendt
Affiliation:
General Electric Company, Corporate Research and Development P. O. Box 8, Schenectady, NY 12301
M. F. Garbauskas
Affiliation:
General Electric Company, Corporate Research and Development P. O. Box 8, Schenectady, NY 12301
L. L. Schilling
Affiliation:
General Electric Company, Corporate Research and Development P. O. Box 8, Schenectady, NY 12301
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Abstract

Results are presented on efforts to prepare both the 80K, Bi2CaSr2Cu2Oz (2122), and 11 OK, (Bi,Pb)2Ca2Sr2Cu3Oz (2223), transition temperature bismuth superconducting species in either phase pure or nearly phase pure, powdered form using either equimolar NaCI-KCI or NaBiOz as molten fluxes. Data are presented on the effects of variation of the reaction temperature and duration, solvent content, relative CaO and CuO contents, and of post-synthesis anneals of the product materials.

Type
Research Article
Copyright
Copyright © Materials Research Society 1990

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References

1 Agostinelli, E., Bohandy, J., Green, W. J., Phillips, T. E., Kim, B. F., Adrian, F. J., Moorjani, K., J. Mater. Res. 4 (5), 1103(1989).CrossRefGoogle Scholar
2 Arendt, R. H., Garbauskas, M. F., Schilling, L. L., J. Mater. Res., in press.Google Scholar
3 Arendt, R. H., J. Solid State Chem. 8, 339(1973).CrossRefGoogle Scholar
4 Arendt, R. H., Pasco, W. D., J. Electrochem. Soc. 134 [3], 733 (1987).CrossRefGoogle Scholar

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