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Carbon Onion Films-Molecular Interactions of Multi-Layer Fullerenes

Published online by Cambridge University Press:  31 January 2011

Raed A. Alduhaileb
Affiliation:
alduhail@msu.edu, Michigan State University, East Lansing, Michigan, United States
Virginia M. Ayres
Affiliation:
ayresv@msu.edu, Michigan State University, East Lansing, Michigan, United States
Benjamin W. Jacobs
Affiliation:
bjacobs@sandia.gov, Michigan State University, East Lansing, Michigan, United States
Xudong Fan
Affiliation:
fanx@msu.edu, Michigan State University, East Lansing, Michigan, United States
Kaylee McElroy
Affiliation:
kaylees@gmail.com, Michigan State University, East Lansing, Michigan, United States
Martin Crimp
Affiliation:
crimp@egr.msu.edu, Michigan State University, East Lansing, Michigan, United States
Atsushi Hirata
Affiliation:
ahirata@ctrl.titech.ac.jp, Tokyo Institute of Technology, Tokyo, Japan
Mutsumi Horikoshi
Affiliation:
miwa@se.ctrl.titech.ac.jp, Tokyo Institute of Technology, Tokyo, Japan
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Abstract

The evolution of carbon onion structure from spherical to polyhedral is correlated with changes in the sp3/sp2 ratio as a function of increasing synthesis temperature using electron energy loss spectroscopy, scanning electron microscopy, and high resolution electron microscopy. Results that are obtained using asymmetric f-variance versus symmetric Gaussian deconvolution of electron energy loss spectra are compared. The possibility of a separate peak at 287 eV is discussed.

Type
Research Article
Copyright
Copyright © Materials Research Society 2010

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References

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5. Brydson, R., Zhili, Z. and Brown, A., “Revisiting the Determination of Carbon sp3/sp2 Ratios via Analysis of the EELS Carbon K-edge,” EMC 2008: Vol 1: Instrumentation and Methods, edited by Luysberg, M., Tillmann, K. and Weirich, T. (Springer-Verlag, Berlin, Germany, 2008) pp. 357358.Google Scholar
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