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In Situ X-Ray Diffraction Studies of Crystallization Growth Behavior in ZnO-Bi2O3-B2O3 Glass as a Route to Functional Optical Devices

  • Quentin Altemose (a1), Katrina Raichle (a1), Brittani Schnable (a1), Casey Schwarz (a1), Myungkoo Kang (a2), Carlo Pantano (a3), Kathleen Richardson (a2) and Clara Rivero-Baleine (a4)...

Abstract

Transparent optical ZnO–Bi2O3–B2O3 (ZBB) glass-ceramics were created by the melt quenching technique. In this work, a melt of the glass containing stoichiometric ratios of Zn/Bi/B and As was studied. Differential scanning calorimeter (DSC) measurements was used to measure the thermal behavior. VIS/NIR transmission measurements were used to determine the transmission window. X-ray diffraction (XRD) was used to determine crystal phase. In this study, we explore new techniques and report a detailed study of in-situ XRD of the ZBB composition in order to correlate nucleation temperature, heat treatment temperature, and heat treatment duration with induced crystal phase.

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1.Raichle, K., Schnable, B., Altemose, Q., Schwarz, C., Kang, M., Pantano, C., Richardson, K. and Rivero-Baleine, C., presented at the APS Conferences for Undergraduate Women in Physics Princeton, New Jersey, 2017 (unpublished).
2.Shanmugalevu, B. and Kumar, V.V., J. Am. Ceram. Soc., 85, 9, 28912898, (2012).
3.Zeng, H., Liu, Z., Jiang, Q., Li, B., Yang, C., Shang, Z., Ren, J. and Chen, G., J. Eur. Ceram. Soc., 34, 16, (2014).

Keywords

In Situ X-Ray Diffraction Studies of Crystallization Growth Behavior in ZnO-Bi2O3-B2O3 Glass as a Route to Functional Optical Devices

  • Quentin Altemose (a1), Katrina Raichle (a1), Brittani Schnable (a1), Casey Schwarz (a1), Myungkoo Kang (a2), Carlo Pantano (a3), Kathleen Richardson (a2) and Clara Rivero-Baleine (a4)...

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