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Correlating Atom Probe Crystallographic Measurements with Transmission Kikuchi Diffraction Data

  • Andrew J. Breen (a1) (a2), Katharina Babinsky (a3), Alec C. Day (a1) (a2), K. Eder (a1) (a2), Connor J. Oakman (a1) (a2), Patrick W. Trimby (a1), Sophie Primig (a4), Julie M. Cairney (a1) and Simon P. Ringer (a1) (a2) (a5)...

Abstract

Correlative microscopy approaches offer synergistic solutions to many research problems. One such combination, that has been studied in limited detail, is the use of atom probe tomography (APT) and transmission Kikuchi diffraction (TKD) on the same tip specimen. By combining these two powerful microscopy techniques, the microstructure of important engineering alloys can be studied in greater detail. For the first time, the accuracy of crystallographic measurements made using APT will be independently verified using TKD. Experimental data from two atom probe tips, one a nanocrystalline Al–0.5Ag alloy specimen collected on a straight flight-path atom probe and the other a high purity Mo specimen collected on a reflectron-fitted instrument, will be compared. We find that the average minimum misorientation angle, calculated from calibrated atom probe reconstructions with two different pole combinations, deviate 0.7° and 1.4°, respectively, from the TKD results. The type of atom probe and experimental conditions appear to have some impact on this accuracy and the reconstruction and measurement procedures are likely to contribute further to degradation in angular resolution. The challenges and implications of this correlative approach will also be discussed.

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Araullo-Peters, V.J., Breen, A., Ceguerra, A.V., Gault, B., Ringer, S.P. & Cairney, J.M. (2015). A new systematic framework for crystallographic analysis of atom probe data. Ultramicroscopy 154(0), 714.
Araullo-Peters, V.J., Gault, B., Shrestha, S.L., Yao, L., Moody, M.P., Ringer, S.P. & Cairney, J.M. (2012). Atom probe crystallography: Atomic-scale 3-D orientation mapping. Scr Mater 66(11), 907910.
Babinsky, K., De Kloe, R., Clemens, H. & Primig, S. (2014 a). A novel approach for site-specific atom probe specimen preparation by focused ion beam and transmission electron backscatter diffraction. Ultramicroscopy 144, 918.
Babinsky, K., Weidow, J., Knabl, W., Lorich, A., Leitner, H. & Primig, S. (2014 b). Atom probe study of grain boundary segregation in technically pure molybdenum. Mater Charact 87, 95103.
Breen, A.J., Moody, M.P., Ceguerra, A.V., Gault, B., Araullo-Peters, V.J. & Ringer, S.P. (2015). Restoring the lattice of Si-based atom probe reconstructions for enhanced information on dopant positioning. Ultramicroscopy 159, 314323.
Gault, B., Loi, S.T., Araullo-Peters, V.J., Stephenson, L.T., Moody, M.P., Shrestha, S.L., Marceau, R.K.W., Yao, L., Cairney, J.M. & Ringer, S.P. (2011). Dynamic reconstruction for atom probe tomography. Ultramicroscopy 111(11), 16191624.
Gault, B., Moody, M.P., Cairney, J.M. & Ringer, S.P. (2012 a). Atom probe crystallography. Mater Today 15(9), 378386.
Gault, B., Moody, M.P., Cairney, J.M. & Ringer, S.P. (2012 b). Atom Probe Microscopy. New York: Springer.
Gault, B., Moody, M.P., de Geuser, F., Tsafnat, G., La Fontaine, A., Stephenson, L.T., Haley, D. & Ringer, S.P. (2009). Advances in the calibration of atom probe tomographic reconstruction. J Appl Phys 105(3), 034913.
He, M.R., Samudrala, S.K., Kim, G., Felfer, P.J., Breen, A.J., Cairney, J.M. & Gianola, D.S. (2016). Linking stress-driven microstructural evolution in nanocrystalline aluminium with grain boundary doping of oxygen. Nat Commun 7, article no. 11225.
Herbig, M., Choi, P. & Raabe, D. (2015). Combining structural and chemical information at the nanometer scale by correlative transmission electron microscopy and atom probe tomography. Ultramicroscopy 153, 3239.
Herbig, M., Raabe, D., Li, Y., Choi, P., Zaefferer, S. & Goto, S. (2014). Atomic-scale quantification of grain boundary segregation in nanocrystalline material. Phys Rev Lett 112(12), 126103.
Keller, R. & Geiss, R. (2012). Transmission EBSD from 10 nm domains in a scanning electron microscope. J Microsc 245(3), 245251.
Larson, D.J., Prosa, T.J., Ulfig, R.M., Geiser, B.P. & Kelly, T.F. (2013). Local Electrode Atom Probe Tomography. New York: Springer Science.
Liddicoat, P.V., Liao, X.-Z., Zhao, Y., Zhu, Y., Murashkin, M.Y., Lavernia, E.J., Valiev, R.Z. & Ringer, S.P. (2010). Nanostructural hierarchy increases the strength of aluminium alloys. Nat Commun 1, 63.
Miller, M.K., Cerezo, A., Hetherington, M. & Smith, G.D.W. (1996). Atom Probe Field Ion Microscopy. Oxford, UK: Oxford Science Publications, Clarendon Press.
Miller, M.K. & Forbes, R.G. (2014). Atom-Probe Tomography – The Local Electrode Atom Probe. London, UK: Springer.
Moody, M.P., Ceguerra, A.V., Breen, A.J., Cui, X.Y., Gault, B., Stephenson, L.T., Marceau, R.K.W., Powles, R.C. & Ringer, S.P. (2014). Atomically resolved tomography to directly inform simulations for structure–property relationships. Nat Commun 5, article no. 5501.
Moody, M.P., Gault, B., Stephenson, L.T., Haley, D. & Ringer, S.P. (2009). Qualification of the tomographic reconstruction in atom probe by advanced spatial distribution map techniques. Ultramicroscopy 109(7), 815824.
Primig, S., Clemens, H., Knabl, W., Lorich, A. & Stickler, R. (2015). Orientation dependent recovery and recrystallization behavior of hot-rolled molybdenum. Int J Refract Metals Hard Mater 48, 179186.
Prior, D.J. (1999). Problems in determining the misorientation axes, for small angular misorientations, using electron backscatter diffraction in the SEM. J Microsc 195(3), 217225.
Randle, V. & Engler, O. (2000). Introduction to Texture Analysis: Macrotexture, Microtexture and Orientation Mapping. Amsterdam: Gordon & Breach.
Rice, K.P., Chen, Y., Prosa, T.J. & Larson, D.J. (2016). Implementing transmission electron backscatter diffraction for atom probe tomography. Microsc Microanal 22(3), 583588.
Rohrer, G.S. (2011). Grain boundary energy anisotropy: A review. J Mater Sci 46(18), 58815895.
Takahashi, J., Kawakami, K. & Kobayashi, Y. (2014). In situ determination of misorientation angle of grain boundary by field ion microscopy analysis. Ultramicroscopy 140, 2025.
Trimby, P.W. (2012). Orientation mapping of nanostructured materials using transmission Kikuchi diffraction in the scanning electron microscope. Ultramicroscopy 120, 1624.
Trimby, P.W., Cao, Y., Chen, Z., Han, S., Hemker, K.J., Lian, J., Liao, X., Rottmann, P., Samudrala, S., Sun, J., Wang, J.T., Wheeler, J. & Cairney, J.M. (2014). Characterizing deformed ultrafine-grained and nanocrystalline materials using transmission Kikuchi diffraction in a scanning electron microscope. Acta Mater 62, 6980.
Vurpillot, F., Da Costa, G., Menand, A. & Blavette, D. (2001). Structural analyses in three-dimensional atom probe: A Fourier transform approach. J Microsc 203(3), 295302.
Vurpillot, F., Renaud, L. & Blavette, D. (2003). A new step towards the lattice reconstruction in 3DAP. Ultramicroscopy 95, 223229.
Yao, L. (2016). A filtering method to reveal crystalline patterns from atom probe microscopy desorption maps. MethodsX 3, 268273.
Yao, L., Ringer, S.P., Cairney, J.M. & Miller, M.K. (2013). The anatomy of grain boundaries: Their structure and atomic-level solute distribution. Scr Mater 69(8), 622625.
Yen, H.-W., Ooi, S.W., Eizadjou, M., Breen, A., Huang, C.-Y., Bhadeshia, H. & Ringer, S.P. (2015). Role of stress-assisted martensite in the design of strong ultrafine-grained duplex steels. Acta Mater 82, 100114.
Zaefferer, S. (2011). A critical review of orientation microscopy in SEM and TEM. Cryst Res Technol 46(6), 607628.

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Correlating Atom Probe Crystallographic Measurements with Transmission Kikuchi Diffraction Data

  • Andrew J. Breen (a1) (a2), Katharina Babinsky (a3), Alec C. Day (a1) (a2), K. Eder (a1) (a2), Connor J. Oakman (a1) (a2), Patrick W. Trimby (a1), Sophie Primig (a4), Julie M. Cairney (a1) and Simon P. Ringer (a1) (a2) (a5)...

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