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The Basics of Microtomy for Materials Science Microscopy

Published online by Cambridge University Press:  02 July 2020

Tom Malis*
Affiliation:
Materials Technology Laboratory, 568 Booth St. Ottawa, CanadaK1A 0G1 (http://malis@nrcan.gc.ca)
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Extract

The common theme of most forms of thin specimen preparation for the physical sciences has been the controlled, gradual removal of material, whether by electrolytic dissolution, ion bombardment, careful mechanical dimpling or step-by-step tripod polishing. It is somewhat ironic that a “brute force” method, wherein the material is forced at a high rate against an atomically sharp diamond wedge so that an ultrathin slice, or section, is sheared, or fractured, from a ‘block’ of the material, should be viewed not only as acceptable, but with growing enthusiasm in the last several years. This process, known as ultramicrotomy, originated in life science TEM, but has been modified by materials scientists and applied to an impressive array of materials as illustrated in Table 1, culminating, perhaps, with the recent successful sectioning of diamond film.

Type
Tem Specimen Preparation in the Physical Sciences
Copyright
Copyright © Microscopy Society of America

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References

References:

1.Malis, T. and Steele, D., Spec. Prep, for TEM of Materials, MRS Symp., 199 (1990) 3.CrossRefGoogle Scholar
2.Swab, P., Microscopy Research and Techniques, 31 (1995) 308.CrossRefGoogle Scholar