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Adaptive Orientation Imaging Microscopy

Published online by Cambridge University Press:  02 July 2020

W. Yang
Affiliation:
Department of Materials Science & Engineering, Carnegie Mellon University, Pittsburgh, PA15213
C.-T. Wu
Affiliation:
Department of Materials Science & Engineering, Carnegie Mellon University, Pittsburgh, PA15213
B.L. Adams
Affiliation:
Department of Materials Science & Engineering, Carnegie Mellon University, Pittsburgh, PA15213
M. De Graef
Affiliation:
Department of Materials Science & Engineering, Carnegie Mellon University, Pittsburgh, PA15213
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Extract

This paper describes a new form of orientation imaging microscopy: Adaptive Orientation Imaging Microscopy or AOIM. In standard OIM experiments the local orientation of the crystal lattice is determined with respect to a suitable reference frame by acquiring and indexing electron back-scattering (EBS) patterns on a square or hexagonal grid of sampling points. Since its invention, OIM has been extensively used to characterize polycrystalline materials. With the fast development of computers and CCD camera systems in the past few years, the standard OIM can now acquire and index of the order of 4000 EBS patterns per hour.

In a typical OIM experiment one is usually interested in either the overall texture of. the sample, or in the types and relative frequencies of grain boundaries. In the former case the proper way of acquiring orientation data involves the use of an equidistant grid of sampling points. In the latter case, however, a large fraction of the acquisition time is wasted sampling the grain interior, which does not provide any information about the grain boundaries.

Type
Electron diffraction in the SEM: automated EBSP and its application
Copyright
Copyright © Microscopy Society of America

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References

references

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4 This work is supported by the MRSEC Program of the NSF under Award Number DMR-9632556.Google Scholar