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Surface-oxidation studies of cube-textured, pure nickel to form NiO as a potential YBa2Cu3O7−x-coated conductor buffer layer

Published online by Cambridge University Press:  31 January 2011

Z. Lockman ,
A. Berenov ,
W. Goldacker ,
R. Nast ,
B. deBoer ,
B. Holzapfel  and
J.L. MacManus-Driscoll
Z. Lockman
Affiliation:
Department of Materials, Imperial College, Prince Consort Road, London, SW7 2BP, United Kingdom
A. Berenov
Affiliation:
Department of Materials, Imperial College, Prince Consort Road, London, SW7 2BP, United Kingdom
W. Goldacker
Affiliation:
Forschungszentrum Karlsruhe, Techniqk und Umwelt, Institut for Festkorperforschung, Hermann-von-Helmholtz-Platz-1, D-7634 Eggenstein-Leopoldshafen, Germany
R. Nast
Affiliation:
Forschungszentrum Karlsruhe, Techniqk und Umwelt, Institut for Festkorperforschung, Hermann-von-Helmholtz-Platz-1, D-7634 Eggenstein-Leopoldshafen, Germany
B. deBoer
Affiliation:
Institut für Festkörper- und Werkstofforschung, D-01171 Dresden, Germany
B. Holzapfel
Affiliation:
Institut für Festkörper- und Werkstofforschung, D-01171 Dresden, Germany
J.L. MacManus-Driscoll
Affiliation:
Department of Materials, Imperial College, Prince Consort Road, London, SW7 2BP, United Kingdom
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Abstract

The growth of nickel oxide (NiO) on {100}〈001〉 cube textured, rolling-assisted biaxially textured substrates (RABiTS) of pure nickel was studied. Single-phase (100) NiO formed only in a narrow temperature range at 1250 ± 5 °C. At lower or higher temperatures, other orientations, namely (111), (311), and (220), also formed. At 1250 °C, practically single phase (100) NiO was observed for short oxidation times t of 0.2–10 min (oxide thickness < 10 μm). For 10 < t < 120 min, small quantities of (111) NiO formed in addition to (100), but near-single-phase (100) NiO formed once again after oxidation for >150 min (thickness > 35 μm). The ratio of (100) to (111) textures with oxidation time is explained in terms of epitaxial constraints, growth rates, and oxygen absorption on the (100) and (111) grains. The optimum oxidation conditions are oxidation for approximately 0.5 min at 1250 °C in flowing oxygen, yielding (100) NiO, a few microns in thickness, and root-mean-square roughness of approximately 40 nm on the length-scale of the grain size.

Type
Articles
Information
Journal of Materials Research , Volume 18 , Issue 2 , February 2003 , pp. 327 - 337
Copyright
Copyright © Materials Research Society 2003

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References

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