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Hydrothermal synthesis and characterization of a new potassium phosphatoantimonate

Published online by Cambridge University Press:  03 March 2011

Yonglin An ,
Shouhua Feng ,
Yihua Xu ,
Ruren Xu  and
Yong Yue
Yonglin An
Affiliation:
Key Laboratory of Inorganic Hydrothermal Synthesis, Jilin University, Changchun 130023, People's Republic of China
Shouhua Feng
Affiliation:
Key Laboratory of Inorganic Hydrothermal Synthesis, Jilin University, Changchun 130023, People's Republic of China
Yihua Xu
Affiliation:
Key Laboratory of Inorganic Hydrothermal Synthesis, Jilin University, Changchun 130023, People's Republic of China
Ruren Xu
Affiliation:
Key Laboratory of Inorganic Hydrothermal Synthesis, Jilin University, Changchun 130023, People's Republic of China
Yong Yue
Affiliation:
Wuhan Institute of Physics, Academia Sinica, Wuhan 430071, People's Republic of China
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Abstract

A new potassium phosphatoantimonate with a composition of 4K2O · 4Sb2O5 · P2O5 · 8H2O, which crystallizes in a monoclinic system with a = 23.952 Å, b = 9.515 Å, c = 8.193 Å, and β = 124.77, was hydrothermally synthesized and characterized by powder x-ray diffraction, chemical composition analysis, x-ray photoelectron spectroscopy, and 31P MAS-NMR techniques. The potassium ion can be exchanged by other monovalent ions.

Type
Rapid Communications
Information
Journal of Materials Research , Volume 9 , Issue 11 , November 1994 , pp. 2745 - 2746
Copyright
Copyright © Materials Research Society 1994

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References

REFERENCES

1Piffard, Y., Lachgar, A., and Tournoux, M., Mater. Res. Bull. XX, 715 (1985).Google Scholar
2Piffard, Y., Lachgar, A., and Tournoux, M., J. Solid State Chem. 58, 253 (1985).CrossRefGoogle Scholar
3Piffard, Y., Oyetola, S., Courant, M., and Lachgar, A., J. Solid State Chem. 60, 209 (1985).CrossRefGoogle Scholar
4Piffard, Y., Oyetola, S., Verbarere, A., and Tournoux, M., J. Solid State Chem. 63, 81 (1986).CrossRefGoogle Scholar
5Lachgar, A., Deniard-Dourant, S., and Piffard, Y., J. Solid State Chem. 63, 409 (1986).Google Scholar
6Piffard, Y., Lachgar, A., and Tournoux, M., Mater. Res. Bull. XXI, 1231 (1986).Google Scholar
7Greenblatt, M. and Wang, E., Chem. Mater. 3 (3), 542 (1991).Google Scholar
8Greenblatt, M. and Wang, E., Chem. Mater. 3 (4), 703 (1991).Google Scholar
9Taulelle, F., Sanchez, C., Livage, J., Lachgar, A., and Piffard, Y., J. Phys. Chem. Solids 49 (3), 299 (1988).Google Scholar