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Combustion synthesis method for synthesis of aluminum nitride powder using aluminum containers

Published online by Cambridge University Press:  31 January 2011

Chun-Nan Lin  and
Shyan-Lung Chung
Chun-Nan Lin
Affiliation:
Department of Chemical Engineering, National Cheng Kung University, Tainan, Taiwan, 70101, Republic of China
Shyan-Lung Chung*
Affiliation:
Department of Chemical Engineering, National Cheng Kung University, Tainan, Taiwan, 70101, Republic of China
*
a)Address all correspondence to this author. e-mail: slchung@mail.ncku.edu.tw
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Abstract

A combustion synthesis method was developed for synthesis of AlN powder. Al powder and small amounts of NH4Cl were thoroughly mixed and placed in low-melting-point containers made of a thin, perforated aluminum sheet. The combustion reaction was ignited by heating the top surface of the powder stack, and the aluminum container was converted completely to AlN during the combustion reaction. High product yields were obtained under N2 pressures of 0.2–0.5 MPa. The product was composed of a dense outer portion and a loose inner portion. Effects of several process parameters on the product yield were investigated and discussed.

Type
Articles
Information
Journal of Materials Research , Volume 16 , Issue 12 , December 2001 , pp. 3518 - 3525
Copyright
Copyright © Materials Research Society 2001

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