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Effect of annealing on magnetic properties of Ni–Mn–Ga glass-coated microwires

Published online by Cambridge University Press:  11 May 2018

Arcady Zhukov Open the ORCID record for Arcady Zhukov [Opens in a new window] ,
Mihail Ipatov ,
Juan J. del Val ,
Paula Corte-León ,
Julian Gonzalez ,
Alexandr Granovsky  and
Valentina Zhukova
Arcady Zhukov*
Affiliation:
Departamento de Física de Materiales, UPV/EHU, San Sebastián 20018, Spain; Departamento de Física Aplicada, EUPDS, UPV/EHU, San Sebastian 20018, Spain; and IKERBASQUE, Basque Foundation for Science, Bilbao 48011, Spain
Mihail Ipatov
Affiliation:
Departamento de Física de Materiales, UPV/EHU, San Sebastián 20018, Spain; and IKERBASQUE, Basque Foundation for Science, Bilbao 48011, Spain
Juan J. del Val
Affiliation:
Departamento de Física de Materiales, UPV/EHU, San Sebastián 20018, Spain
Paula Corte-León
Affiliation:
Departamento de Física de Materiales, UPV/EHU, San Sebastián 20018, Spain; and Departamento de Física Aplicada, EUPDS, UPV/EHU, San Sebastian 20018, Spain
Julian Gonzalez
Affiliation:
Departamento de Física de Materiales, UPV/EHU, San Sebastián 20018, Spain
Alexandr Granovsky
Affiliation:
Faculty of Physics, Lomonosov Moscow State University, Moscow 11991, Russian Federation
Valentina Zhukova
Affiliation:
Departamento de Física de Materiales, UPV/EHU, San Sebastián 20018, Spain
*
a)Address all correspondence to this author. e-mail: arkadi.joukov@ehu.es
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Abstract

We studied the effect of annealing on magnetic properties and structure of Heusler-type NiMnGa glass-covered microwires with a metallic nucleus diameter of about 22 μm prepared using the Taylor–Ulitovsky method. The as-prepared NiMnGa glass-covered microwires do not present ferromagnetic order at room temperature. Magnetization curves of the as-prepared samples do not present either saturation or coercivity at temperatures above 5 K. After annealing of the microwires, a ferromagnetic ordering is obtained with a Curie temperature of about 300 K which is beneficial for magnetic solid state refrigeration. The hysteresis observed on temperature dependence of magnetization in annealed samples and magnetic softening at about 260 K has been interpreted as the first-order phase transformation. Observed changes have been discussed considering internal stress relaxation after annealing, nanocrystalline structure of the as-prepared and annealed samples, recrystallization process and magnetic ordering of phases identified in the as-prepared sample and appearing under recrystallization. Existence of insulating and flexible glass-coating is beneficial for improvement of mechanical properties but the glass coating considerably affects magnetic properties of NiMnGa microwires. Therefore special attention must be paid to annealing conditions for realization of martensitic transformation.

Keywords

Heusler alloysannealingglass-coated microwires
Type
Article
Information
Journal of Materials Research , Volume 33 , Issue 15: Focus Issue: Soft Magnetic Materials: Synthesis, Characterization, and Applications , 13 August 2018 , pp. 2148 - 2155
Copyright
Copyright © Materials Research Society 2018 

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