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Observations on the heat-induced salt balance changes in milk II. Reversibility on cooling

Published online by Cambridge University Press:  01 June 2009

Yves Pouliot
Affiliation:
Groupe de Recherche STELA, Département de Sciences et Technologie des Aliments, Université Laval, Québec, CanadaG1K 7P4
Marcel Boulet
Affiliation:
Groupe de Recherche STELA, Département de Sciences et Technologie des Aliments, Université Laval, Québec, CanadaG1K 7P4
Paul Paquin
Affiliation:
Groupe de Recherche STELA, Département de Sciences et Technologie des Aliments, Université Laval, Québec, CanadaG1K 7P4

Summary

Milk which had been heated to 85°C for 40 min was examined for changes to milk salts taking place upon cooling to 4, 20, 40 and 60°C. The time-concentration curves showed a two-step reaction for Ca, Pi and pH. The effect of the heat treatment in milk heated to 85°C for 40 min was to produce greater changes in the second step of the reaction. Because of the variability of the results for other species (Mg and citrate), the reversibility was calculated only for Ca and P. It was 90–95% and 93–99% respectively depending on the cooling temperature. The reversibility of the heat-induced changes and especially of the possible dissolution equilibrium between Ca phosphate and citrate precipitates on cooling are discussed.

Type
Original Articles
Copyright
Copyright © Proprietors of Journal of Dairy Research 1989

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References

REFERENCES

Allen, R. J. 1940 The determination of phosphorus. Biochemical Journal 34 858865CrossRefGoogle Scholar
Boulet, M. 1966 Formation of calcium phosphate in milk and milk ultrafiltrate. 17th International Dairy Congress, Munich B 111118Google Scholar
Boulet, M. & Marier, J. R. 1960 Solubility of tricalcium citrate in solutions of variable ionic strength and in milk ultrafiltrates. Journal of Dairy Science 43 155164CrossRefGoogle Scholar
Brooks, I. B., Luster, G. A. & Easterly, D. G. 1970 A procedure for the rapid determination of the major cations in milk by atomic absorption spectrophotometry. Atomic Absorption Newsletter 9 93Google Scholar
Davies, D. T. & White, J. C. D. 1959 Determination of heat-induced changes in the protein stability and chemical composition of milk. 15th International Dairy Congress, London 3 16771684Google Scholar
Eanes, E. D. & Meyer, J. L. 1977 The maturation of crystalline calcium phosphates in aqueous suspensions at physiologic pH. Calcified Tissue Research 23 259263CrossRefGoogle ScholarPubMed
Hilgeman, M. & Jenness, R. 1951 Observations on the effect of heat treatment upon the dissolved calcium and phosphorus in skimmilk. Journal of Dairy Science 34 483484Google Scholar
Kannan, A. & Jenness, R. 1961 Relation of milk serum proteins and milk salts to the effects of heat treatment on rennet clotting. Journal of Dairy Science 44 808822CrossRefGoogle Scholar
Kocak, H. R., Zadow, J. G. & Purcell, J. 1984 Short term changes in the ionic calcium content of the heat-treated skim milk. Australian Journal of Dairy Technology 39 4043Google Scholar
Kuramoto, S., Jenness, R., Coulter, S. T. & Choi, R. P. 1959 Standardization of the Harland-Ashworth test for whey protein nitrogen. Journal of Dairy Science 42 2838CrossRefGoogle Scholar
Marier, J. R. & Boulet, M. 1958 Direct determination of citric acid in milk with an improved pryridine-acetic anhydride method. Journal of Dairy Science 41 16831692CrossRefGoogle Scholar
Morrissey, P. A. 1969 The rennet hysteresis of heated milk. Journal of Dairy Research 36 333341CrossRefGoogle Scholar
Muldoon, P. J. & Liska, B. J. 1972 Effects of heat treatment and subsequent storage on the concentration of ionized calcium in skimmilk. Journal of Dairy Science 55 3538CrossRefGoogle Scholar
Pouliot, Y., Boulet, M. & Paquin, P. 1989 a An experimental technique for the study of salt balance in milk. Journal of Dairy Science In pressCrossRefGoogle Scholar
Pouliot, Y., Boulet, M. & Paquin, P. 1989 b Observations on the heat-induced salt balance changes in milk. I. Effect of heating time 4 and 90°C. Journal of Dairy Research 56 185192CrossRefGoogle Scholar
Rose, D. & Tessier, H. 1959 Composition of ultrafiltrates from milk heated at 80 to 230°F, in relation to heat stability. Journal of Dairy Science 42 969980CrossRefGoogle Scholar
Schmidt, D. G. & Both, P. 1987 Studies on the precipitation of calcium phosphate. I. Experiments in the pH range 5·3 to 6·8 at 25°C and 50°C in the absence of additives. Netherlands Milk and Dairy Journal 41 105120Google Scholar
Verma, I. S. & Sommer, H. H. 1958 Effect of pasteurization and cool-aging on the salt balance of milk. Journal of Dairy Science 41 914919.CrossRefGoogle Scholar